(E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide

The title compound, C(12)H(9)FN(2)O(2), was prepared by the reaction of 2-fluoro­benzaldehyde and furan-2-carbohydrazide. The furan ring is disordered over two sets of sites with refined occupancies of 0.60 (3):0.40 (3). The major and minor components of the furan ring make dihedral angles of 51.9 (...

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Autor principal: Jiang, Jin-He
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051579/
https://www.ncbi.nlm.nih.gov/pubmed/21522934
http://dx.doi.org/10.1107/S1600536810052980
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author Jiang, Jin-He
author_facet Jiang, Jin-He
author_sort Jiang, Jin-He
collection PubMed
description The title compound, C(12)H(9)FN(2)O(2), was prepared by the reaction of 2-fluoro­benzaldehyde and furan-2-carbohydrazide. The furan ring is disordered over two sets of sites with refined occupancies of 0.60 (3):0.40 (3). The major and minor components of the furan ring make dihedral angles of 51.9 (6) and 38.0 (10)°, respectively, with the benzene ring. In the crystal, mol­ecules are linked via bifurcated N—H⋯O(N) hydrogen bonds into chains along [001].
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spelling pubmed-30515792011-04-26 (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide Jiang, Jin-He Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(9)FN(2)O(2), was prepared by the reaction of 2-fluoro­benzaldehyde and furan-2-carbohydrazide. The furan ring is disordered over two sets of sites with refined occupancies of 0.60 (3):0.40 (3). The major and minor components of the furan ring make dihedral angles of 51.9 (6) and 38.0 (10)°, respectively, with the benzene ring. In the crystal, mol­ecules are linked via bifurcated N—H⋯O(N) hydrogen bonds into chains along [001]. International Union of Crystallography 2011-01-08 /pmc/articles/PMC3051579/ /pubmed/21522934 http://dx.doi.org/10.1107/S1600536810052980 Text en © Jin-He Jiang 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jiang, Jin-He
(E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title_full (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title_fullStr (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title_full_unstemmed (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title_short (E)-N′-(2-Fluoro­benzyl­idene)furan-2-carbohydrazide
title_sort (e)-n′-(2-fluoro­benzyl­idene)furan-2-carbohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051579/
https://www.ncbi.nlm.nih.gov/pubmed/21522934
http://dx.doi.org/10.1107/S1600536810052980
work_keys_str_mv AT jiangjinhe en2fluorobenzylidenefuran2carbohydrazide

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