1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione

In the title compound, C(13)H(15)ClN(2)S, the dihydro­pyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydro­pyrimidine and benzene rings is 86.62 (13)°. The crystal stru...

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Detalles Bibliográficos
Autores principales: Yamin, Bohari M., Salem, Halima Farag
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051597/
https://www.ncbi.nlm.nih.gov/pubmed/21522974
http://dx.doi.org/10.1107/S1600536810054292
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author Yamin, Bohari M.
Salem, Halima Farag
author_facet Yamin, Bohari M.
Salem, Halima Farag
author_sort Yamin, Bohari M.
collection PubMed
description In the title compound, C(13)H(15)ClN(2)S, the dihydro­pyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydro­pyrimidine and benzene rings is 86.62 (13)°. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds, which form centrosymmetric dimers arranged along the c axis.
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spelling pubmed-30515972011-04-26 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione Yamin, Bohari M. Salem, Halima Farag Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(15)ClN(2)S, the dihydro­pyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydro­pyrimidine and benzene rings is 86.62 (13)°. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds, which form centrosymmetric dimers arranged along the c axis. International Union of Crystallography 2011-01-08 /pmc/articles/PMC3051597/ /pubmed/21522974 http://dx.doi.org/10.1107/S1600536810054292 Text en © Yamin and Salem 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yamin, Bohari M.
Salem, Halima Farag
1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title_full 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title_fullStr 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title_full_unstemmed 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title_short 1-(3-Chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
title_sort 1-(3-chloro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051597/
https://www.ncbi.nlm.nih.gov/pubmed/21522974
http://dx.doi.org/10.1107/S1600536810054292
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