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3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide

The title compound, C(14)H(10)Cl(2)N(2)O, was prepared from the reaction of 2-chloro­benzaldehyde with 3-chloro­benzo­hydrazide in methanol. The mol­ecule adopts an E configuration about the methyl­idene unit and the two aromatic rings form a dihedral angle of 13.8 (2)°. In the crystal, mol­ecules a...

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Detalles Bibliográficos
Autores principales: Lei, Yan, Fu, Chuan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051651/
https://www.ncbi.nlm.nih.gov/pubmed/21523081
http://dx.doi.org/10.1107/S1600536811001656
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author Lei, Yan
Fu, Chuan
author_facet Lei, Yan
Fu, Chuan
author_sort Lei, Yan
collection PubMed
description The title compound, C(14)H(10)Cl(2)N(2)O, was prepared from the reaction of 2-chloro­benzaldehyde with 3-chloro­benzo­hydrazide in methanol. The mol­ecule adopts an E configuration about the methyl­idene unit and the two aromatic rings form a dihedral angle of 13.8 (2)°. In the crystal, mol­ecules are linked via inter­molecular N—H⋯O and C—H⋯O hydrogen bonds, forming chains along the c axis.
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spelling pubmed-30516512011-04-26 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide Lei, Yan Fu, Chuan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(10)Cl(2)N(2)O, was prepared from the reaction of 2-chloro­benzaldehyde with 3-chloro­benzo­hydrazide in methanol. The mol­ecule adopts an E configuration about the methyl­idene unit and the two aromatic rings form a dihedral angle of 13.8 (2)°. In the crystal, mol­ecules are linked via inter­molecular N—H⋯O and C—H⋯O hydrogen bonds, forming chains along the c axis. International Union of Crystallography 2011-01-15 /pmc/articles/PMC3051651/ /pubmed/21523081 http://dx.doi.org/10.1107/S1600536811001656 Text en © Lei and Fu 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lei, Yan
Fu, Chuan
3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title_full 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title_fullStr 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title_full_unstemmed 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title_short 3-Chloro-N′-(2-chloro­benzyl­idene)benzohydrazide
title_sort 3-chloro-n′-(2-chloro­benzyl­idene)benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051651/
https://www.ncbi.nlm.nih.gov/pubmed/21523081
http://dx.doi.org/10.1107/S1600536811001656
work_keys_str_mv AT leiyan 3chloron2chlorobenzylidenebenzohydrazide
AT fuchuan 3chloron2chlorobenzylidenebenzohydrazide