5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione

In the title compound, C(13)H(11)ClN(2)O(6), the dihedral angles between the benzene ring and the amino­methyl­ene unit and between the amino­methyl­ene group and the dioxane ring are 8.19 (14) and 1.39 (17)°, respectively. The dioxane ring has a half-boat conformation, in which the C atom between t...

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Detalles Bibliográficos
Autores principales: Lan, Xian-Qiu, Zhang, Xiao-Feng, Yang, Ying-Hong, Luo, You-Fu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051652/
https://www.ncbi.nlm.nih.gov/pubmed/21523065
http://dx.doi.org/10.1107/S160053681100095X
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author Lan, Xian-Qiu
Zhang, Xiao-Feng
Yang, Ying-Hong
Luo, You-Fu
author_facet Lan, Xian-Qiu
Zhang, Xiao-Feng
Yang, Ying-Hong
Luo, You-Fu
author_sort Lan, Xian-Qiu
collection PubMed
description In the title compound, C(13)H(11)ClN(2)O(6), the dihedral angles between the benzene ring and the amino­methyl­ene unit and between the amino­methyl­ene group and the dioxane ring are 8.19 (14) and 1.39 (17)°, respectively. The dioxane ring has a half-boat conformation, in which the C atom between the dioxane O atoms is 0.662 (4)Å out of the plane through the remaining ring atoms. Intra­molecular N—H⋯O and N—H⋯Cl inter­actions occur.
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spelling pubmed-30516522011-04-26 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione Lan, Xian-Qiu Zhang, Xiao-Feng Yang, Ying-Hong Luo, You-Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(11)ClN(2)O(6), the dihedral angles between the benzene ring and the amino­methyl­ene unit and between the amino­methyl­ene group and the dioxane ring are 8.19 (14) and 1.39 (17)°, respectively. The dioxane ring has a half-boat conformation, in which the C atom between the dioxane O atoms is 0.662 (4)Å out of the plane through the remaining ring atoms. Intra­molecular N—H⋯O and N—H⋯Cl inter­actions occur. International Union of Crystallography 2011-01-15 /pmc/articles/PMC3051652/ /pubmed/21523065 http://dx.doi.org/10.1107/S160053681100095X Text en © Lan et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lan, Xian-Qiu
Zhang, Xiao-Feng
Yang, Ying-Hong
Luo, You-Fu
5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title_full 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title_fullStr 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title_full_unstemmed 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title_short 5-[(2-Chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
title_sort 5-[(2-chloro-4-nitro­anilino)methyl­idene]-2,2-dimethyl-1,3-dioxane-4,6-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051652/
https://www.ncbi.nlm.nih.gov/pubmed/21523065
http://dx.doi.org/10.1107/S160053681100095X
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AT luoyoufu 52chloro4nitroanilinomethylidene22dimethyl13dioxane46dione

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