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3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide
The title compound, C(18)H(13)ClN(2)O(2), was prepared by the reaction of 2-hydroxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. An intramolecular O—H⋯N hydrogen bond influences the molecular conformation; the benzene ring and naphthyl ring system form a dihedral angle of 17.1 (3)°....
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051679/ https://www.ncbi.nlm.nih.gov/pubmed/21523050 http://dx.doi.org/10.1107/S1600536811000912 |
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author | Li, Tian-Yi Li, Wei |
author_facet | Li, Tian-Yi Li, Wei |
author_sort | Li, Tian-Yi |
collection | PubMed |
description | The title compound, C(18)H(13)ClN(2)O(2), was prepared by the reaction of 2-hydroxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. An intramolecular O—H⋯N hydrogen bond influences the molecular conformation; the benzene ring and naphthyl ring system form a dihedral angle of 17.1 (3)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains propagated in [101]. |
format | Text |
id | pubmed-3051679 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30516792011-04-26 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide Li, Tian-Yi Li, Wei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(13)ClN(2)O(2), was prepared by the reaction of 2-hydroxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. An intramolecular O—H⋯N hydrogen bond influences the molecular conformation; the benzene ring and naphthyl ring system form a dihedral angle of 17.1 (3)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains propagated in [101]. International Union of Crystallography 2011-01-12 /pmc/articles/PMC3051679/ /pubmed/21523050 http://dx.doi.org/10.1107/S1600536811000912 Text en © Li and Li 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Li, Tian-Yi Li, Wei 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title | 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title_full | 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title_fullStr | 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title_full_unstemmed | 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title_short | 3-Chloro-N′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
title_sort | 3-chloro-n′-[(2-hydroxynaphthalen-1-yl)methylidene]benzohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051679/ https://www.ncbi.nlm.nih.gov/pubmed/21523050 http://dx.doi.org/10.1107/S1600536811000912 |
work_keys_str_mv | AT litianyi 3chloron2hydroxynaphthalen1ylmethylidenebenzohydrazide AT liwei 3chloron2hydroxynaphthalen1ylmethylidenebenzohydrazide |