3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate

The title Schiff base compound, C(14)H(9)Br(2)ClN(2)O(2)·CH(3)OH, features an intra­molecular O—H⋯N hydrogen bond, which contributes to the planarity of the mol­ecule: the dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, pairs of adjacent mol­ecules are linked through inter­...

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Detalles Bibliográficos
Autores principales: Li, Tian-Yi, Qu, Yue-Gang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051720/
https://www.ncbi.nlm.nih.gov/pubmed/21523014
http://dx.doi.org/10.1107/S1600536811000742
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author Li, Tian-Yi
Qu, Yue-Gang
author_facet Li, Tian-Yi
Qu, Yue-Gang
author_sort Li, Tian-Yi
collection PubMed
description The title Schiff base compound, C(14)H(9)Br(2)ClN(2)O(2)·CH(3)OH, features an intra­molecular O—H⋯N hydrogen bond, which contributes to the planarity of the mol­ecule: the dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, pairs of adjacent mol­ecules are linked through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds, forming dimers. The methanol solvent mol­ecule is linked by inter­molecular O—H⋯O hydrogen bonds.
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spelling pubmed-30517202011-04-26 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate Li, Tian-Yi Qu, Yue-Gang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title Schiff base compound, C(14)H(9)Br(2)ClN(2)O(2)·CH(3)OH, features an intra­molecular O—H⋯N hydrogen bond, which contributes to the planarity of the mol­ecule: the dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, pairs of adjacent mol­ecules are linked through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds, forming dimers. The methanol solvent mol­ecule is linked by inter­molecular O—H⋯O hydrogen bonds. International Union of Crystallography 2011-01-12 /pmc/articles/PMC3051720/ /pubmed/21523014 http://dx.doi.org/10.1107/S1600536811000742 Text en © Li and Qu 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Tian-Yi
Qu, Yue-Gang
3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_fullStr 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full_unstemmed 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_short 3-Chloro-N′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_sort 3-chloro-n′-(3,5-dibromo-2-hy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051720/
https://www.ncbi.nlm.nih.gov/pubmed/21523014
http://dx.doi.org/10.1107/S1600536811000742
work_keys_str_mv AT litianyi 3chloron35dibromo2hydroxybenzylidenebenzohydrazidemethanolmonosolvate
AT quyuegang 3chloron35dibromo2hydroxybenzylidenebenzohydrazidemethanolmonosolvate

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