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3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide
The title compound, C(19)H(15)ClN(2)O(2), was prepared by the reaction of 2-methoxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. The dihedral angle between the benzene ring and the naphthyl ring system is 69.0 (3)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecu...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2011
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051782/ https://www.ncbi.nlm.nih.gov/pubmed/21523051 http://dx.doi.org/10.1107/S1600536811000924 |
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author | Li, Tian-Yi Ge, Yan-Xia |
author_facet | Li, Tian-Yi Ge, Yan-Xia |
author_sort | Li, Tian-Yi |
collection | PubMed |
description | The title compound, C(19)H(15)ClN(2)O(2), was prepared by the reaction of 2-methoxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. The dihedral angle between the benzene ring and the naphthyl ring system is 69.0 (3)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the c axis. The crystal packing exhibits π–π interactions, as indicated by distances of 3.768 (3) Å between the centroids of the naphthyl rings of neighbouring molecules. |
format | Text |
id | pubmed-3051782 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30517822011-04-26 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide Li, Tian-Yi Ge, Yan-Xia Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(15)ClN(2)O(2), was prepared by the reaction of 2-methoxy-1-naphthaldehyde with 3-chlorobenzohydrazide in methanol. The dihedral angle between the benzene ring and the naphthyl ring system is 69.0 (3)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the c axis. The crystal packing exhibits π–π interactions, as indicated by distances of 3.768 (3) Å between the centroids of the naphthyl rings of neighbouring molecules. International Union of Crystallography 2011-01-12 /pmc/articles/PMC3051782/ /pubmed/21523051 http://dx.doi.org/10.1107/S1600536811000924 Text en © Li and Ge 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Li, Tian-Yi Ge, Yan-Xia 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title | 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title_full | 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title_fullStr | 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title_full_unstemmed | 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title_short | 3-Chloro-N′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
title_sort | 3-chloro-n′-[(2-methoxynaphthalen-1-yl)methylidene]benzohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051782/ https://www.ncbi.nlm.nih.gov/pubmed/21523051 http://dx.doi.org/10.1107/S1600536811000924 |
work_keys_str_mv | AT litianyi 3chloron2methoxynaphthalen1ylmethylidenebenzohydrazide AT geyanxia 3chloron2methoxynaphthalen1ylmethylidenebenzohydrazide |