[(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate

In the title compound, C(9)H(11)N(3)O·CH(4)O, the semicarbazone moiety is nearly planar [maximum deviation = 0.017 (2) Å] and is twisted by a dihedral angle of 29.40 (13)° with respect to the phenyl ring. The semicarbazone moiety and phenyl ring are located on opposite sides of the C=N bond, showing...

Descripción completa

Detalles Bibliográficos
Autores principales: Liu, Guang-Bin, Chen, Peng-Sheng, Liu, Chang-Xiang, Fu, Ling, Nie, Xu-Liang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051788/
https://www.ncbi.nlm.nih.gov/pubmed/21523026
http://dx.doi.org/10.1107/S1600536811000225
_version_ 1782199562433200128
author Liu, Guang-Bin
Chen, Peng-Sheng
Liu, Chang-Xiang
Fu, Ling
Nie, Xu-Liang
author_facet Liu, Guang-Bin
Chen, Peng-Sheng
Liu, Chang-Xiang
Fu, Ling
Nie, Xu-Liang
author_sort Liu, Guang-Bin
collection PubMed
description In the title compound, C(9)H(11)N(3)O·CH(4)O, the semicarbazone moiety is nearly planar [maximum deviation = 0.017 (2) Å] and is twisted by a dihedral angle of 29.40 (13)° with respect to the phenyl ring. The semicarbazone moiety and phenyl ring are located on opposite sides of the C=N bond, showing the E configuration. An inter­molecular O—H⋯O and N—H⋯O hydrogen-bonding network occurs in the crystal structure.
format Text
id pubmed-3051788
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-30517882011-04-26 [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate Liu, Guang-Bin Chen, Peng-Sheng Liu, Chang-Xiang Fu, Ling Nie, Xu-Liang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(11)N(3)O·CH(4)O, the semicarbazone moiety is nearly planar [maximum deviation = 0.017 (2) Å] and is twisted by a dihedral angle of 29.40 (13)° with respect to the phenyl ring. The semicarbazone moiety and phenyl ring are located on opposite sides of the C=N bond, showing the E configuration. An inter­molecular O—H⋯O and N—H⋯O hydrogen-bonding network occurs in the crystal structure. International Union of Crystallography 2011-01-12 /pmc/articles/PMC3051788/ /pubmed/21523026 http://dx.doi.org/10.1107/S1600536811000225 Text en © Liu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Guang-Bin
Chen, Peng-Sheng
Liu, Chang-Xiang
Fu, Ling
Nie, Xu-Liang
[(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title_full [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title_fullStr [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title_full_unstemmed [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title_short [(E)-(1-Phenyl­ethyl­idene)amino]­urea methanol monosolvate
title_sort [(e)-(1-phenyl­ethyl­idene)amino]­urea methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051788/
https://www.ncbi.nlm.nih.gov/pubmed/21523026
http://dx.doi.org/10.1107/S1600536811000225
work_keys_str_mv AT liuguangbin e1phenylethylideneaminoureamethanolmonosolvate
AT chenpengsheng e1phenylethylideneaminoureamethanolmonosolvate
AT liuchangxiang e1phenylethylideneaminoureamethanolmonosolvate
AT fuling e1phenylethylideneaminoureamethanolmonosolvate
AT niexuliang e1phenylethylideneaminoureamethanolmonosolvate

Ejemplares similares