Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin

In the title compound, C(16)H(14)N(2)O(5), a non-merohedral twin, the dihedral angle between the mean planes of the two benzene rings is 4.0 (9)°. The ethyl group is disordered [0.643 (14) and 0.357 (14) occupancy]. The nitro group is twisted by 16.4 (4)° from the mean plane of the benzene ring and...

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Autores principales: Saeed, Sohail, Rashid, Naghmana, Jasinski, Jerry P., Butcher, Ray J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051796/
https://www.ncbi.nlm.nih.gov/pubmed/21523125
http://dx.doi.org/10.1107/S1600536811002236
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author Saeed, Sohail
Rashid, Naghmana
Jasinski, Jerry P.
Butcher, Ray J.
author_facet Saeed, Sohail
Rashid, Naghmana
Jasinski, Jerry P.
Butcher, Ray J.
author_sort Saeed, Sohail
collection PubMed
description In the title compound, C(16)H(14)N(2)O(5), a non-merohedral twin, the dihedral angle between the mean planes of the two benzene rings is 4.0 (9)°. The ethyl group is disordered [0.643 (14) and 0.357 (14) occupancy]. The nitro group is twisted by 16.4 (4)° from the mean plane of the benzene ring and the mean plane of the carbonyl group is twisted from the mean planes of the two benzene rings by 4.5 (0) and 4.7 (9)°. An intra­molecular N—H⋯O hydrogen bond occurs. The crystal packing is stabilized by weak inter­molecular C—H⋯O hydrogen-bond inter­actions.
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spelling pubmed-30517962011-04-26 Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin Saeed, Sohail Rashid, Naghmana Jasinski, Jerry P. Butcher, Ray J. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(14)N(2)O(5), a non-merohedral twin, the dihedral angle between the mean planes of the two benzene rings is 4.0 (9)°. The ethyl group is disordered [0.643 (14) and 0.357 (14) occupancy]. The nitro group is twisted by 16.4 (4)° from the mean plane of the benzene ring and the mean plane of the carbonyl group is twisted from the mean planes of the two benzene rings by 4.5 (0) and 4.7 (9)°. An intra­molecular N—H⋯O hydrogen bond occurs. The crystal packing is stabilized by weak inter­molecular C—H⋯O hydrogen-bond inter­actions. International Union of Crystallography 2011-01-22 /pmc/articles/PMC3051796/ /pubmed/21523125 http://dx.doi.org/10.1107/S1600536811002236 Text en © Saeed et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Sohail
Rashid, Naghmana
Jasinski, Jerry P.
Butcher, Ray J.
Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title_full Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title_fullStr Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title_full_unstemmed Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title_short Ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
title_sort ethyl 2-(4-nitro­benzamido)­benzoate, a non-merohedral twin
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051796/
https://www.ncbi.nlm.nih.gov/pubmed/21523125
http://dx.doi.org/10.1107/S1600536811002236
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AT butcherrayj ethyl24nitrobenzamidobenzoateanonmerohedraltwin

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