Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide

There are two molecules in the asymmetric unit of the title compound, C(24)H(22)N(2)O(4)S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C—H⋯O...

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Detalles Bibliográficos
Autores principales: Bassin, Jatinder P., Shah, Virender P., Martin, Lee, Horton, Peter N.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052004/
https://www.ncbi.nlm.nih.gov/pubmed/21522430
http://dx.doi.org/10.1107/S1600536811004983
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author Bassin, Jatinder P.
Shah, Virender P.
Martin, Lee
Horton, Peter N.
author_facet Bassin, Jatinder P.
Shah, Virender P.
Martin, Lee
Horton, Peter N.
author_sort Bassin, Jatinder P.
collection PubMed
description There are two molecules in the asymmetric unit of the title compound, C(24)H(22)N(2)O(4)S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C—H⋯O hydrogen bonds.
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spelling pubmed-30520042011-04-26 Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide Bassin, Jatinder P. Shah, Virender P. Martin, Lee Horton, Peter N. Acta Crystallogr Sect E Struct Rep Online Organic Papers There are two molecules in the asymmetric unit of the title compound, C(24)H(22)N(2)O(4)S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C—H⋯O hydrogen bonds. International Union of Crystallography 2011-02-23 /pmc/articles/PMC3052004/ /pubmed/21522430 http://dx.doi.org/10.1107/S1600536811004983 Text en © Bassin et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bassin, Jatinder P.
Shah, Virender P.
Martin, Lee
Horton, Peter N.
Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title_full Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title_fullStr Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title_full_unstemmed Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title_short Racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
title_sort racemic 9,10-dimeth­oxy-3-methyl-6-phenyl-7,7a-dihydro­benzo[b]benzo[4,5]isothia­zolo[2,3-d][1,4]diazepine 12,12-dioxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052004/
https://www.ncbi.nlm.nih.gov/pubmed/21522430
http://dx.doi.org/10.1107/S1600536811004983
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AT martinlee racemic910dimethoxy3methyl6phenyl77adihydrobenzobbenzo45isothiazolo23d14diazepine1212dioxide
AT hortonpetern racemic910dimethoxy3methyl6phenyl77adihydrobenzobbenzo45isothiazolo23d14diazepine1212dioxide

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