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3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline

In the crystal structure of the title compound, C(30)H(24)N(4)O(2)S, the dihydro­quinoxaline fused-ring system is disordered over three orientations in a 0.358 (2):0.318 (3):0.324 (3) ratio; the mean planes of the non-H atoms of the disorder components are aligned at 4.0 (3), 11.8 (4) and 41.7 (2)°...

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Detalles Bibliográficos
Autores principales: Abdel-Aziz, Hatem A., Bari, Ahmed, Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052037/
https://www.ncbi.nlm.nih.gov/pubmed/21522440
http://dx.doi.org/10.1107/S1600536811005940
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author Abdel-Aziz, Hatem A.
Bari, Ahmed
Ng, Seik Weng
author_facet Abdel-Aziz, Hatem A.
Bari, Ahmed
Ng, Seik Weng
author_sort Abdel-Aziz, Hatem A.
collection PubMed
description In the crystal structure of the title compound, C(30)H(24)N(4)O(2)S, the dihydro­quinoxaline fused-ring system is disordered over three orientations in a 0.358 (2):0.318 (3):0.324 (3) ratio; the mean planes of the non-H atoms of the disorder components are aligned at 4.0 (3), 11.8 (4) and 41.7 (2)° with respect to the pyrazole ring. The rings of the phenyl and tolyl substituents are aligned at 64.0 (1) and 43.7 (1)° with respect to the pyrazole ring. Weak intermolecular C—H⋯O hydrogen bonding links the mol­ecules, forming supra­molecular chains running along the a axis.
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spelling pubmed-30520372011-04-26 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline Abdel-Aziz, Hatem A. Bari, Ahmed Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(30)H(24)N(4)O(2)S, the dihydro­quinoxaline fused-ring system is disordered over three orientations in a 0.358 (2):0.318 (3):0.324 (3) ratio; the mean planes of the non-H atoms of the disorder components are aligned at 4.0 (3), 11.8 (4) and 41.7 (2)° with respect to the pyrazole ring. The rings of the phenyl and tolyl substituents are aligned at 64.0 (1) and 43.7 (1)° with respect to the pyrazole ring. Weak intermolecular C—H⋯O hydrogen bonding links the mol­ecules, forming supra­molecular chains running along the a axis. International Union of Crystallography 2011-02-23 /pmc/articles/PMC3052037/ /pubmed/21522440 http://dx.doi.org/10.1107/S1600536811005940 Text en © Abdel-Aziz et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Abdel-Aziz, Hatem A.
Bari, Ahmed
Ng, Seik Weng
3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title_full 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title_fullStr 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title_full_unstemmed 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title_short 3-(5-Phenyl-4-phenyl­sulfonyl-1-p-tolyl-1H-pyrazol-3-yl)-1,2-dihydro­quinoxaline
title_sort 3-(5-phenyl-4-phenyl­sulfonyl-1-p-tolyl-1h-pyrazol-3-yl)-1,2-dihydro­quinoxaline
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052037/
https://www.ncbi.nlm.nih.gov/pubmed/21522440
http://dx.doi.org/10.1107/S1600536811005940
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