(E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime

In the title compound, C(13)H(11)ClN(2)O(3), the nine-membered bicycle includes an oxime group having the C=N group in an E configuration. The isoxazole ring is almost planar [r.m.s. deviation = 0.0056 Å]; the dihedral angle between the isoxazole and 4-chloro­phenyl ring is 75.60 (5)°. In the crysta...

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Detalles Bibliográficos
Autores principales: Lim, Hyun Sub, Kim, Hyung Jin, Otgonbaatar, Enkhzul, Kwak, Chee-Hun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052067/
https://www.ncbi.nlm.nih.gov/pubmed/21522420
http://dx.doi.org/10.1107/S1600536811005575
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author Lim, Hyun Sub
Kim, Hyung Jin
Otgonbaatar, Enkhzul
Kwak, Chee-Hun
author_facet Lim, Hyun Sub
Kim, Hyung Jin
Otgonbaatar, Enkhzul
Kwak, Chee-Hun
author_sort Lim, Hyun Sub
collection PubMed
description In the title compound, C(13)H(11)ClN(2)O(3), the nine-membered bicycle includes an oxime group having the C=N group in an E configuration. The isoxazole ring is almost planar [r.m.s. deviation = 0.0056 Å]; the dihedral angle between the isoxazole and 4-chloro­phenyl ring is 75.60 (5)°. In the crystal, inter­molecular O—H⋯N(isoxazole) hydrogen bonds give rise to chains running along the b axis.
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spelling pubmed-30520672011-04-26 (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime Lim, Hyun Sub Kim, Hyung Jin Otgonbaatar, Enkhzul Kwak, Chee-Hun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(11)ClN(2)O(3), the nine-membered bicycle includes an oxime group having the C=N group in an E configuration. The isoxazole ring is almost planar [r.m.s. deviation = 0.0056 Å]; the dihedral angle between the isoxazole and 4-chloro­phenyl ring is 75.60 (5)°. In the crystal, inter­molecular O—H⋯N(isoxazole) hydrogen bonds give rise to chains running along the b axis. International Union of Crystallography 2011-02-19 /pmc/articles/PMC3052067/ /pubmed/21522420 http://dx.doi.org/10.1107/S1600536811005575 Text en © Kim et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lim, Hyun Sub
Kim, Hyung Jin
Otgonbaatar, Enkhzul
Kwak, Chee-Hun
(E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title_full (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title_fullStr (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title_full_unstemmed (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title_short (E)-7-(4-Chloro­phen­yl)-5,7-dihydro-4H-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
title_sort (e)-7-(4-chloro­phen­yl)-5,7-dihydro-4h-pyrano[3,4-c]isoxazole-3-carbaldehyde oxime
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052067/
https://www.ncbi.nlm.nih.gov/pubmed/21522420
http://dx.doi.org/10.1107/S1600536811005575
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AT otgonbaatarenkhzul e74chlorophenyl57dihydro4hpyrano34cisoxazole3carbaldehydeoxime
AT kwakcheehun e74chlorophenyl57dihydro4hpyrano34cisoxazole3carbaldehydeoxime

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