3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one

In the title compound, C(20)H(12)F(2)N(2)O(4), the two benzene rings of the tricyclic unit are oriented at a dihedral angle of 30.6 (1)°. The 2,4-difluoro­anilino residue is oriented at a dihedral angle of 68.2 (1)° with respect to the phen­oxy ring. In the crystal, N—H⋯O hydrogen bonds between the...

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Detalles Bibliográficos
Autores principales: Baur, Benjamin, Schollmeyer, Dieter, Laufer, Stefan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052073/
https://www.ncbi.nlm.nih.gov/pubmed/21522320
http://dx.doi.org/10.1107/S1600536811002881
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author Baur, Benjamin
Schollmeyer, Dieter
Laufer, Stefan
author_facet Baur, Benjamin
Schollmeyer, Dieter
Laufer, Stefan
author_sort Baur, Benjamin
collection PubMed
description In the title compound, C(20)H(12)F(2)N(2)O(4), the two benzene rings of the tricyclic unit are oriented at a dihedral angle of 30.6 (1)°. The 2,4-difluoro­anilino residue is oriented at a dihedral angle of 68.2 (1)° with respect to the phen­oxy ring. In the crystal, N—H⋯O hydrogen bonds between the amino group and the carbonyl O atom of the oxepinone ring link the mol­ecules into infinte chains along the c axis.
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spelling pubmed-30520732011-04-26 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one Baur, Benjamin Schollmeyer, Dieter Laufer, Stefan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(12)F(2)N(2)O(4), the two benzene rings of the tricyclic unit are oriented at a dihedral angle of 30.6 (1)°. The 2,4-difluoro­anilino residue is oriented at a dihedral angle of 68.2 (1)° with respect to the phen­oxy ring. In the crystal, N—H⋯O hydrogen bonds between the amino group and the carbonyl O atom of the oxepinone ring link the mol­ecules into infinte chains along the c axis. International Union of Crystallography 2011-02-02 /pmc/articles/PMC3052073/ /pubmed/21522320 http://dx.doi.org/10.1107/S1600536811002881 Text en © Baur et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Baur, Benjamin
Schollmeyer, Dieter
Laufer, Stefan
3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title_full 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title_fullStr 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title_full_unstemmed 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title_short 3-(2,4-Difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6H)-one
title_sort 3-(2,4-difluoro­anilino)-9-nitro­dibenzo[b,e]oxepin-11(6h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052073/
https://www.ncbi.nlm.nih.gov/pubmed/21522320
http://dx.doi.org/10.1107/S1600536811002881
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