6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine

The title compound, C(11)H(6)ClN(5)O(4)S, crystallized with two independent mol­ecules in the asymmetric unit. The benzene ring makes dihedral angles of 66.46 (8) and 85.77 (9)° with the mean plane of the purine ring in the two mol­ecules. In the crystal, inter­molecular π–π stacking inter­actions [...

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Detalles Bibliográficos
Autores principales: Wang, Ning-Yu, Deng, Mei, Xia, Yong, Yu, Luo-Ting
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052074/
https://www.ncbi.nlm.nih.gov/pubmed/21522432
http://dx.doi.org/10.1107/S1600536811003102
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author Wang, Ning-Yu
Deng, Mei
Xia, Yong
Yu, Luo-Ting
author_facet Wang, Ning-Yu
Deng, Mei
Xia, Yong
Yu, Luo-Ting
author_sort Wang, Ning-Yu
collection PubMed
description The title compound, C(11)H(6)ClN(5)O(4)S, crystallized with two independent mol­ecules in the asymmetric unit. The benzene ring makes dihedral angles of 66.46 (8) and 85.77 (9)° with the mean plane of the purine ring in the two mol­ecules. In the crystal, inter­molecular π–π stacking inter­actions [centroid–centroid distance = 3.8968 (12) Å], C—Cl⋯π inter­actions [Cl⋯centroid = 3.2505 (10) Å, C—Cl⋯centroid = 161.56 (18)°] and non-classical C—H⋯O and C—H⋯N hydrogen bonds link the molecules.
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spelling pubmed-30520742011-04-26 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine Wang, Ning-Yu Deng, Mei Xia, Yong Yu, Luo-Ting Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(6)ClN(5)O(4)S, crystallized with two independent mol­ecules in the asymmetric unit. The benzene ring makes dihedral angles of 66.46 (8) and 85.77 (9)° with the mean plane of the purine ring in the two mol­ecules. In the crystal, inter­molecular π–π stacking inter­actions [centroid–centroid distance = 3.8968 (12) Å], C—Cl⋯π inter­actions [Cl⋯centroid = 3.2505 (10) Å, C—Cl⋯centroid = 161.56 (18)°] and non-classical C—H⋯O and C—H⋯N hydrogen bonds link the molecules. International Union of Crystallography 2011-02-23 /pmc/articles/PMC3052074/ /pubmed/21522432 http://dx.doi.org/10.1107/S1600536811003102 Text en © Wang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Ning-Yu
Deng, Mei
Xia, Yong
Yu, Luo-Ting
6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title_full 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title_fullStr 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title_full_unstemmed 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title_short 6-Chloro-9-(2-nitro­phenyl­sulfon­yl)-9H-purine
title_sort 6-chloro-9-(2-nitro­phenyl­sulfon­yl)-9h-purine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052074/
https://www.ncbi.nlm.nih.gov/pubmed/21522432
http://dx.doi.org/10.1107/S1600536811003102
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AT dengmei 6chloro92nitrophenylsulfonyl9hpurine
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