3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate

In the title compound, C(10)H(6)N(4)O(5)S·H(2)O, the thia­zole ring is twisted at a dihedral angle of 25.87 (7)° with respect to the benzene ring. The water mol­ecule is linked with the benzamide mol­ecules via N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds. In the crystal, π–π stacking is observed between n...

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Detalles Bibliográficos
Autores principales: Saeed, Sohail, Rashid, Naghmana, Wong, Wing-Tak, Hussain, Rizwan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052084/
https://www.ncbi.nlm.nih.gov/pubmed/21522411
http://dx.doi.org/10.1107/S1600536811005228
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author Saeed, Sohail
Rashid, Naghmana
Wong, Wing-Tak
Hussain, Rizwan
author_facet Saeed, Sohail
Rashid, Naghmana
Wong, Wing-Tak
Hussain, Rizwan
author_sort Saeed, Sohail
collection PubMed
description In the title compound, C(10)H(6)N(4)O(5)S·H(2)O, the thia­zole ring is twisted at a dihedral angle of 25.87 (7)° with respect to the benzene ring. The water mol­ecule is linked with the benzamide mol­ecules via N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds. In the crystal, π–π stacking is observed between nearly parallel [dihedral angle = 7.02 (7)°] thia­zole and benzene rings of adjacent mol­ecules, the centroid–centroid distances being 3.7107 (9) and 3.7158 (9) Å, respectively.
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spelling pubmed-30520842011-04-26 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate Saeed, Sohail Rashid, Naghmana Wong, Wing-Tak Hussain, Rizwan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(6)N(4)O(5)S·H(2)O, the thia­zole ring is twisted at a dihedral angle of 25.87 (7)° with respect to the benzene ring. The water mol­ecule is linked with the benzamide mol­ecules via N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds. In the crystal, π–π stacking is observed between nearly parallel [dihedral angle = 7.02 (7)°] thia­zole and benzene rings of adjacent mol­ecules, the centroid–centroid distances being 3.7107 (9) and 3.7158 (9) Å, respectively. International Union of Crystallography 2011-02-19 /pmc/articles/PMC3052084/ /pubmed/21522411 http://dx.doi.org/10.1107/S1600536811005228 Text en © Saeed et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Sohail
Rashid, Naghmana
Wong, Wing-Tak
Hussain, Rizwan
3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title_full 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title_fullStr 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title_full_unstemmed 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title_short 3,5-Dinitro-N-(1,3-thia­zol-2-yl)benzamide monohydrate
title_sort 3,5-dinitro-n-(1,3-thia­zol-2-yl)benzamide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052084/
https://www.ncbi.nlm.nih.gov/pubmed/21522411
http://dx.doi.org/10.1107/S1600536811005228
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AT hussainrizwan 35dinitron13thiazol2ylbenzamidemonohydrate

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