5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine

The title compound, C(14)H(13)BrN(2)O, was obtained by reaction of indan-1-yl methane­sulfonate with 2-amino-5-bromo­pyridin-3-ol in the presence of caesium carbonate. The indane ring system is approximately planar [all but one of the C atoms are coplanar within 0.03 Å, the latter atom being displac...

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Detalles Bibliográficos
Autores principales: Cho-Schultz, Sujin, Kath, John C., Moore, Curtis, Rheingold, Arnold L., Yanovsky, Alex
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052095/
https://www.ncbi.nlm.nih.gov/pubmed/21522402
http://dx.doi.org/10.1107/S1600536811005332
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author Cho-Schultz, Sujin
Kath, John C.
Moore, Curtis
Rheingold, Arnold L.
Yanovsky, Alex
author_facet Cho-Schultz, Sujin
Kath, John C.
Moore, Curtis
Rheingold, Arnold L.
Yanovsky, Alex
author_sort Cho-Schultz, Sujin
collection PubMed
description The title compound, C(14)H(13)BrN(2)O, was obtained by reaction of indan-1-yl methane­sulfonate with 2-amino-5-bromo­pyridin-3-ol in the presence of caesium carbonate. The indane ring system is approximately planar [all but one of the C atoms are coplanar within 0.03 Å, the latter atom being displaced by 0.206 (2) Å from the mean plane through the remaining atoms] and forms a dihedral angle of 58.41 (4)° with the pyridine ring. In the crystal, centrosymmetrically related mol­ecules are linked into dimers by N—H⋯N hydrogen bonds.
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spelling pubmed-30520952011-04-26 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine Cho-Schultz, Sujin Kath, John C. Moore, Curtis Rheingold, Arnold L. Yanovsky, Alex Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)BrN(2)O, was obtained by reaction of indan-1-yl methane­sulfonate with 2-amino-5-bromo­pyridin-3-ol in the presence of caesium carbonate. The indane ring system is approximately planar [all but one of the C atoms are coplanar within 0.03 Å, the latter atom being displaced by 0.206 (2) Å from the mean plane through the remaining atoms] and forms a dihedral angle of 58.41 (4)° with the pyridine ring. In the crystal, centrosymmetrically related mol­ecules are linked into dimers by N—H⋯N hydrogen bonds. International Union of Crystallography 2011-02-19 /pmc/articles/PMC3052095/ /pubmed/21522402 http://dx.doi.org/10.1107/S1600536811005332 Text en © Cho-Schultz et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Cho-Schultz, Sujin
Kath, John C.
Moore, Curtis
Rheingold, Arnold L.
Yanovsky, Alex
5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title_full 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title_fullStr 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title_full_unstemmed 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title_short 5-Bromo-3-(indan-1-yl­oxy)pyridin-2-amine
title_sort 5-bromo-3-(indan-1-yl­oxy)pyridin-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052095/
https://www.ncbi.nlm.nih.gov/pubmed/21522402
http://dx.doi.org/10.1107/S1600536811005332
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AT kathjohnc 5bromo3indan1yloxypyridin2amine
AT moorecurtis 5bromo3indan1yloxypyridin2amine
AT rheingoldarnoldl 5bromo3indan1yloxypyridin2amine
AT yanovskyalex 5bromo3indan1yloxypyridin2amine

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