2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one

In the title compound, C(13)H(9)Br(2)NO(4), the phenyl and 2-nitro­furan rings are linked by a 2,3-dibromo­propanal group, six atoms of which, including a furyl C atom, are disordered over two positions with a site-occupancy ratio of 0.733 (11):0.267 (11). The dihedral angle between the furan [maxim...

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Autores principales: Shahani, Tara, Fun, Hoong-Kun, Nithinchandra, Kalluraya, Balakrishna
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052152/
https://www.ncbi.nlm.nih.gov/pubmed/21522313
http://dx.doi.org/10.1107/S1600536811003552
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author Shahani, Tara
Fun, Hoong-Kun
Nithinchandra,
Kalluraya, Balakrishna
author_facet Shahani, Tara
Fun, Hoong-Kun
Nithinchandra,
Kalluraya, Balakrishna
author_sort Shahani, Tara
collection PubMed
description In the title compound, C(13)H(9)Br(2)NO(4), the phenyl and 2-nitro­furan rings are linked by a 2,3-dibromo­propanal group, six atoms of which, including a furyl C atom, are disordered over two positions with a site-occupancy ratio of 0.733 (11):0.267 (11). The dihedral angle between the furan [maximum deviation = 0.028 (4) Å] and phenyl rings in the major component is 16.9 (3)°. In the minor component, the corresponding values are 0.87 (4) Å and 23.3 (5)°. In the crystal, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into two-dimensional arrays parallel to the ab plane.
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spelling pubmed-30521522011-04-26 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one Shahani, Tara Fun, Hoong-Kun Nithinchandra, Kalluraya, Balakrishna Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(9)Br(2)NO(4), the phenyl and 2-nitro­furan rings are linked by a 2,3-dibromo­propanal group, six atoms of which, including a furyl C atom, are disordered over two positions with a site-occupancy ratio of 0.733 (11):0.267 (11). The dihedral angle between the furan [maximum deviation = 0.028 (4) Å] and phenyl rings in the major component is 16.9 (3)°. In the minor component, the corresponding values are 0.87 (4) Å and 23.3 (5)°. In the crystal, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into two-dimensional arrays parallel to the ab plane. International Union of Crystallography 2011-02-02 /pmc/articles/PMC3052152/ /pubmed/21522313 http://dx.doi.org/10.1107/S1600536811003552 Text en © Shahani et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shahani, Tara
Fun, Hoong-Kun
Nithinchandra,
Kalluraya, Balakrishna
2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title_full 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title_fullStr 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title_full_unstemmed 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title_short 2,3-Dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
title_sort 2,3-dibromo-3-(5-nitro-2-fur­yl)-1-phenyl­propan-1-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3052152/
https://www.ncbi.nlm.nih.gov/pubmed/21522313
http://dx.doi.org/10.1107/S1600536811003552
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AT kallurayabalakrishna 23dibromo35nitro2furyl1phenylpropan1one

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