3-Chloro­pyridin-2-amine

In the title compound, C(5)H(5)ClN(2), a by-product in the synthesis of ethyl 2-(3-chloro­pyridin-2-yl)-5-oxopyrazolidine-3-carboxyl­ate, the amine groups form inter­molecular hydrogen-bonding associations with pyridine N-atom acceptors, giving centrosymmetric cyclic dimers. Short inter­molecular Cl...

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Detalles Bibliográficos
Autores principales: Hu, Zhi-Nan, Yang, Hui-Bin, Luo, Huan, Li, Bin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089079/
https://www.ncbi.nlm.nih.gov/pubmed/21754447
http://dx.doi.org/10.1107/S1600536811013432
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author Hu, Zhi-Nan
Yang, Hui-Bin
Luo, Huan
Li, Bin
author_facet Hu, Zhi-Nan
Yang, Hui-Bin
Luo, Huan
Li, Bin
author_sort Hu, Zhi-Nan
collection PubMed
description In the title compound, C(5)H(5)ClN(2), a by-product in the synthesis of ethyl 2-(3-chloro­pyridin-2-yl)-5-oxopyrazolidine-3-carboxyl­ate, the amine groups form inter­molecular hydrogen-bonding associations with pyridine N-atom acceptors, giving centrosymmetric cyclic dimers. Short inter­molecular Cl⋯Cl inter­actions [3.278 (3) Å] also occur.
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spelling pubmed-30890792011-07-13 3-Chloro­pyridin-2-amine Hu, Zhi-Nan Yang, Hui-Bin Luo, Huan Li, Bin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(5)H(5)ClN(2), a by-product in the synthesis of ethyl 2-(3-chloro­pyridin-2-yl)-5-oxopyrazolidine-3-carboxyl­ate, the amine groups form inter­molecular hydrogen-bonding associations with pyridine N-atom acceptors, giving centrosymmetric cyclic dimers. Short inter­molecular Cl⋯Cl inter­actions [3.278 (3) Å] also occur. International Union of Crystallography 2011-04-16 /pmc/articles/PMC3089079/ /pubmed/21754447 http://dx.doi.org/10.1107/S1600536811013432 Text en © Hu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hu, Zhi-Nan
Yang, Hui-Bin
Luo, Huan
Li, Bin
3-Chloro­pyridin-2-amine
title 3-Chloro­pyridin-2-amine
title_full 3-Chloro­pyridin-2-amine
title_fullStr 3-Chloro­pyridin-2-amine
title_full_unstemmed 3-Chloro­pyridin-2-amine
title_short 3-Chloro­pyridin-2-amine
title_sort 3-chloro­pyridin-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089079/
https://www.ncbi.nlm.nih.gov/pubmed/21754447
http://dx.doi.org/10.1107/S1600536811013432
work_keys_str_mv AT huzhinan 3chloropyridin2amine
AT yanghuibin 3chloropyridin2amine
AT luohuan 3chloropyridin2amine
AT libin 3chloropyridin2amine

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