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(3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one

In the title compound, C(22)H(17)Cl(2)NO(2), the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In th...

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Autores principales: Basiri, Alireza, Murugaiyah, Vikneswaran, Osman, Hasnah, Hemamalini, Madhukar, Fun, Hoong-Kun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089119/
https://www.ncbi.nlm.nih.gov/pubmed/21754526
http://dx.doi.org/10.1107/S1600536811015042
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author Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
author_facet Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
author_sort Basiri, Alireza
collection PubMed
description In the title compound, C(22)H(17)Cl(2)NO(2), the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In the crystal, mol­ecules are connected via weak inter­molecular C—H⋯O hydrogen bonds forming layers perpendicular to the a axis.
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spelling pubmed-30891192011-07-13 (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one Basiri, Alireza Murugaiyah, Vikneswaran Osman, Hasnah Hemamalini, Madhukar Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(22)H(17)Cl(2)NO(2), the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In the crystal, mol­ecules are connected via weak inter­molecular C—H⋯O hydrogen bonds forming layers perpendicular to the a axis. International Union of Crystallography 2011-04-29 /pmc/articles/PMC3089119/ /pubmed/21754526 http://dx.doi.org/10.1107/S1600536811015042 Text en © Basiri et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
(3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_full (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_fullStr (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_full_unstemmed (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_short (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_sort (3e,5e)-1-acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089119/
https://www.ncbi.nlm.nih.gov/pubmed/21754526
http://dx.doi.org/10.1107/S1600536811015042
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