1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea

The title thio­urea derivative, C(14)H(18)N(4)O(5)S, features two substantial twists between its component fragments: the dihedral angle between the SN(2)C (thio­urea) and ONC(2) (amide) residues is 48.89 (7)° and that between the benzene ring and the amide residue is 30.27 (7)°. In the crystal, mol...

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Detalles Bibliográficos
Autores principales: Saeed, Sohail, Rashid, Naghmana, Sher, Muhammad, Ng, Seik Weng, Tiekink, Edward R. T.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089134/
https://www.ncbi.nlm.nih.gov/pubmed/21754469
http://dx.doi.org/10.1107/S1600536811013638
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author Saeed, Sohail
Rashid, Naghmana
Sher, Muhammad
Ng, Seik Weng
Tiekink, Edward R. T.
author_facet Saeed, Sohail
Rashid, Naghmana
Sher, Muhammad
Ng, Seik Weng
Tiekink, Edward R. T.
author_sort Saeed, Sohail
collection PubMed
description The title thio­urea derivative, C(14)H(18)N(4)O(5)S, features two substantial twists between its component fragments: the dihedral angle between the SN(2)C (thio­urea) and ONC(2) (amide) residues is 48.89 (7)° and that between the benzene ring and the amide residue is 30.27 (7)°. In the crystal, mol­ecules are linked by bifurcated N—H⋯(O,S) hydrogen bonds, generating [001] supra­molecular chains.
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spelling pubmed-30891342011-07-13 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea Saeed, Sohail Rashid, Naghmana Sher, Muhammad Ng, Seik Weng Tiekink, Edward R. T. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title thio­urea derivative, C(14)H(18)N(4)O(5)S, features two substantial twists between its component fragments: the dihedral angle between the SN(2)C (thio­urea) and ONC(2) (amide) residues is 48.89 (7)° and that between the benzene ring and the amide residue is 30.27 (7)°. In the crystal, mol­ecules are linked by bifurcated N—H⋯(O,S) hydrogen bonds, generating [001] supra­molecular chains. International Union of Crystallography 2011-04-16 /pmc/articles/PMC3089134/ /pubmed/21754469 http://dx.doi.org/10.1107/S1600536811013638 Text en © Saeed et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Sohail
Rashid, Naghmana
Sher, Muhammad
Ng, Seik Weng
Tiekink, Edward R. T.
1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title_full 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title_fullStr 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title_full_unstemmed 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title_short 1-(3,5-Dinitro­benzo­yl)-3,3-dipropyl­thio­urea
title_sort 1-(3,5-dinitro­benzo­yl)-3,3-dipropyl­thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089134/
https://www.ncbi.nlm.nih.gov/pubmed/21754469
http://dx.doi.org/10.1107/S1600536811013638
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AT ngseikweng 135dinitrobenzoyl33dipropylthiourea
AT tiekinkedwardrt 135dinitrobenzoyl33dipropylthiourea

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