1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine

In the title compound, C(15)H(14)N(4)O(6), the dihedral angle between the aromatic rings is 3.7 (4)°. The nitro groups make dihedral angles of 6.0 (4) and 5.2 (4)° with the parent ring and are oriented at 6.0 (6)° with respect to each other. The meth­oxy groups are inclined at 54.0 (2) and 2.5 (3)°...

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Detalles Bibliográficos
Autores principales: Xin, Xianrong, Li, Min, Chen, Zhimin, Zhu, Ruitao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089222/
https://www.ncbi.nlm.nih.gov/pubmed/21754475
http://dx.doi.org/10.1107/S1600536811013894
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author Xin, Xianrong
Li, Min
Chen, Zhimin
Zhu, Ruitao
author_facet Xin, Xianrong
Li, Min
Chen, Zhimin
Zhu, Ruitao
author_sort Xin, Xianrong
collection PubMed
description In the title compound, C(15)H(14)N(4)O(6), the dihedral angle between the aromatic rings is 3.7 (4)°. The nitro groups make dihedral angles of 6.0 (4) and 5.2 (4)° with the parent ring and are oriented at 6.0 (6)° with respect to each other. The meth­oxy groups are inclined at 54.0 (2) and 2.5 (3)° with respect to the benzene ring to which they are attached. In the crystal, mol­ecules are linked by weak C—H⋯O inter­actions. The mol­ecular conformation is consolidated by an intra­molecular N—H⋯O hydrogen bond.
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spelling pubmed-30892222011-07-13 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine Xin, Xianrong Li, Min Chen, Zhimin Zhu, Ruitao Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(14)N(4)O(6), the dihedral angle between the aromatic rings is 3.7 (4)°. The nitro groups make dihedral angles of 6.0 (4) and 5.2 (4)° with the parent ring and are oriented at 6.0 (6)° with respect to each other. The meth­oxy groups are inclined at 54.0 (2) and 2.5 (3)° with respect to the benzene ring to which they are attached. In the crystal, mol­ecules are linked by weak C—H⋯O inter­actions. The mol­ecular conformation is consolidated by an intra­molecular N—H⋯O hydrogen bond. International Union of Crystallography 2011-04-16 /pmc/articles/PMC3089222/ /pubmed/21754475 http://dx.doi.org/10.1107/S1600536811013894 Text en © Xin et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xin, Xianrong
Li, Min
Chen, Zhimin
Zhu, Ruitao
1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title_full 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title_fullStr 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title_full_unstemmed 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title_short 1-(2,3-Dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
title_sort 1-(2,3-dimeth­oxy­benzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089222/
https://www.ncbi.nlm.nih.gov/pubmed/21754475
http://dx.doi.org/10.1107/S1600536811013894
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AT limin 123dimethoxybenzylidene224dinitrophenylhydrazine
AT chenzhimin 123dimethoxybenzylidene224dinitrophenylhydrazine
AT zhuruitao 123dimethoxybenzylidene224dinitrophenylhydrazine

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