3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea

In the title compound, C(20)H(26)N(2)OS, four non-H atoms of the thio­urea unit are approximately planar (r.m.s. deviation = 0.005 Å); the phenyl and benzene rings are twisted out of this plane by 28.55 (7) and 60.00 (7)°, respectively. An intra­molecular N—H⋯O hydrogen bond occurs. The hy­droxy gro...

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Autores principales: Maharramov, Abel M., Khalilov, Ali N., Sadikhova, Nurlana D., Gurbanov, Atash V., Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089238/
https://www.ncbi.nlm.nih.gov/pubmed/21754408
http://dx.doi.org/10.1107/S1600536811012736
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author Maharramov, Abel M.
Khalilov, Ali N.
Sadikhova, Nurlana D.
Gurbanov, Atash V.
Ng, Seik Weng
author_facet Maharramov, Abel M.
Khalilov, Ali N.
Sadikhova, Nurlana D.
Gurbanov, Atash V.
Ng, Seik Weng
author_sort Maharramov, Abel M.
collection PubMed
description In the title compound, C(20)H(26)N(2)OS, four non-H atoms of the thio­urea unit are approximately planar (r.m.s. deviation = 0.005 Å); the phenyl and benzene rings are twisted out of this plane by 28.55 (7) and 60.00 (7)°, respectively. An intra­molecular N—H⋯O hydrogen bond occurs. The hy­droxy group is hydrogen bonded to the double-bond S atom of an inversion-related mol­ecule, generating a hydrogen-bonded dimer in the crystal structure.
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spelling pubmed-30892382011-07-13 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea Maharramov, Abel M. Khalilov, Ali N. Sadikhova, Nurlana D. Gurbanov, Atash V. Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(26)N(2)OS, four non-H atoms of the thio­urea unit are approximately planar (r.m.s. deviation = 0.005 Å); the phenyl and benzene rings are twisted out of this plane by 28.55 (7) and 60.00 (7)°, respectively. An intra­molecular N—H⋯O hydrogen bond occurs. The hy­droxy group is hydrogen bonded to the double-bond S atom of an inversion-related mol­ecule, generating a hydrogen-bonded dimer in the crystal structure. International Union of Crystallography 2011-04-13 /pmc/articles/PMC3089238/ /pubmed/21754408 http://dx.doi.org/10.1107/S1600536811012736 Text en © Maharramov et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Maharramov, Abel M.
Khalilov, Ali N.
Sadikhova, Nurlana D.
Gurbanov, Atash V.
Ng, Seik Weng
3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title_full 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title_fullStr 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title_full_unstemmed 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title_short 3-[2-Hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
title_sort 3-[2-hy­droxy-3-(2,4,6-trimethyl­phen­yl)prop­yl]-3-methyl-1-phenyl­thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089238/
https://www.ncbi.nlm.nih.gov/pubmed/21754408
http://dx.doi.org/10.1107/S1600536811012736
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AT gurbanovatashv 32hydroxy3246trimethylphenylpropyl3methyl1phenylthiourea
AT ngseikweng 32hydroxy3246trimethylphenylpropyl3methyl1phenylthiourea

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