Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate

In the title compound, C(27)H(23)Cl(3)N(4)O(2), the seven-membered diazepine ring adopts a boat conformation. The triazole ring makes dihedral angles of 17.24 (8) and 82.86 (8)°, respectively, with the chloro­benzene ring and the benzene ring of the benzodiazepine unit.

Detalles Bibliográficos
Autores principales: Boudina, Aicha, Baouid, Abdesselam, Driss, Mohamed, Soumhi, El Hassane
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089256/
https://www.ncbi.nlm.nih.gov/pubmed/21754510
http://dx.doi.org/10.1107/S1600536811014115
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author Boudina, Aicha
Baouid, Abdesselam
Driss, Mohamed
Soumhi, El Hassane
author_facet Boudina, Aicha
Baouid, Abdesselam
Driss, Mohamed
Soumhi, El Hassane
author_sort Boudina, Aicha
collection PubMed
description In the title compound, C(27)H(23)Cl(3)N(4)O(2), the seven-membered diazepine ring adopts a boat conformation. The triazole ring makes dihedral angles of 17.24 (8) and 82.86 (8)°, respectively, with the chloro­benzene ring and the benzene ring of the benzodiazepine unit.
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spelling pubmed-30892562011-07-13 Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate Boudina, Aicha Baouid, Abdesselam Driss, Mohamed Soumhi, El Hassane Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(27)H(23)Cl(3)N(4)O(2), the seven-membered diazepine ring adopts a boat conformation. The triazole ring makes dihedral angles of 17.24 (8) and 82.86 (8)°, respectively, with the chloro­benzene ring and the benzene ring of the benzodiazepine unit. International Union of Crystallography 2011-04-29 /pmc/articles/PMC3089256/ /pubmed/21754510 http://dx.doi.org/10.1107/S1600536811014115 Text en © Boudina et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Boudina, Aicha
Baouid, Abdesselam
Driss, Mohamed
Soumhi, El Hassane
Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title_full Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title_fullStr Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title_full_unstemmed Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title_short Ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3H-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
title_sort ethyl 5,5-dichloro-3-(4-chloro­phen­yl)-3a-methyl-4a-phenyl-3a,4,4a,5-tetra­hydro-3h-aziridino[2,1-d][1,2,4]triazolo[4,3-a][1,5]benzodiazepine-1-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089256/
https://www.ncbi.nlm.nih.gov/pubmed/21754510
http://dx.doi.org/10.1107/S1600536811014115
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