2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate

The title compound, C(13)H(12)N(4)OS·0.5C(3)H(7)NO, contains four hydrazine mol­ecules and two solvent mol­ecules in the asymmetric unit. The dihedral angles between the pyridine and phenyl rings in the hydrazine mol­ecules are 67.51 (16), 68.28 (16), 81.36 (15) and 83.32 (15)°. In the crystal, the...

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Detalles Bibliográficos
Autores principales: Zhao, Pei-Hua, Jiang, Shao-Liang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089371/
https://www.ncbi.nlm.nih.gov/pubmed/21754403
http://dx.doi.org/10.1107/S1600536811011950
Descripción
Sumario:The title compound, C(13)H(12)N(4)OS·0.5C(3)H(7)NO, contains four hydrazine mol­ecules and two solvent mol­ecules in the asymmetric unit. The dihedral angles between the pyridine and phenyl rings in the hydrazine mol­ecules are 67.51 (16), 68.28 (16), 81.36 (15) and 83.32 (15)°. In the crystal, the mol­ecules are linked by N—H⋯N, N—H⋯O and N—H⋯S hydrogen bonds.

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