2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate

The title compound, C(13)H(12)N(4)OS·0.5C(3)H(7)NO, contains four hydrazine mol­ecules and two solvent mol­ecules in the asymmetric unit. The dihedral angles between the pyridine and phenyl rings in the hydrazine mol­ecules are 67.51 (16), 68.28 (16), 81.36 (15) and 83.32 (15)°. In the crystal, the...

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Detalles Bibliográficos
Autores principales: Zhao, Pei-Hua, Jiang, Shao-Liang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089371/
https://www.ncbi.nlm.nih.gov/pubmed/21754403
http://dx.doi.org/10.1107/S1600536811011950
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author Zhao, Pei-Hua
Jiang, Shao-Liang
author_facet Zhao, Pei-Hua
Jiang, Shao-Liang
author_sort Zhao, Pei-Hua
collection PubMed
description The title compound, C(13)H(12)N(4)OS·0.5C(3)H(7)NO, contains four hydrazine mol­ecules and two solvent mol­ecules in the asymmetric unit. The dihedral angles between the pyridine and phenyl rings in the hydrazine mol­ecules are 67.51 (16), 68.28 (16), 81.36 (15) and 83.32 (15)°. In the crystal, the mol­ecules are linked by N—H⋯N, N—H⋯O and N—H⋯S hydrogen bonds.
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spelling pubmed-30893712011-07-13 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate Zhao, Pei-Hua Jiang, Shao-Liang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(12)N(4)OS·0.5C(3)H(7)NO, contains four hydrazine mol­ecules and two solvent mol­ecules in the asymmetric unit. The dihedral angles between the pyridine and phenyl rings in the hydrazine mol­ecules are 67.51 (16), 68.28 (16), 81.36 (15) and 83.32 (15)°. In the crystal, the mol­ecules are linked by N—H⋯N, N—H⋯O and N—H⋯S hydrogen bonds. International Union of Crystallography 2011-04-13 /pmc/articles/PMC3089371/ /pubmed/21754403 http://dx.doi.org/10.1107/S1600536811011950 Text en © Zhao and Jiang 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Pei-Hua
Jiang, Shao-Liang
2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title_full 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title_fullStr 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title_full_unstemmed 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title_short 2-Isonicotinoyl-N-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
title_sort 2-isonicotinoyl-n-phenyl­hydrazine­carbothio­amide dimethyl­formamide hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089371/
https://www.ncbi.nlm.nih.gov/pubmed/21754403
http://dx.doi.org/10.1107/S1600536811011950
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AT jiangshaoliang 2isonicotinoylnphenylhydrazinecarbothioamidedimethylformamidehemisolvate

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