5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)

The aromatic rings of the N,N′-dioxide molecule in the title compound, C(8)H(4)NI(3)O(4)·C(10)H(8)N(2)O(2)·H(2)O, are twisted by 14.0 (2)°. The –CO(2)H substituents of the 5-amino-2,4,6-triiodo­isophthalic acid are twisted by 83.0 (2) and 86.5 (2)° out of the plane of the aromatic ring. In the cryst...

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Detalles Bibliográficos
Autores principales: Zhang, Kou-Lin, Zhang, Jin-Bo, Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099751/
https://www.ncbi.nlm.nih.gov/pubmed/21754083
http://dx.doi.org/10.1107/S1600536811007276
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author Zhang, Kou-Lin
Zhang, Jin-Bo
Ng, Seik Weng
author_facet Zhang, Kou-Lin
Zhang, Jin-Bo
Ng, Seik Weng
author_sort Zhang, Kou-Lin
collection PubMed
description The aromatic rings of the N,N′-dioxide molecule in the title compound, C(8)H(4)NI(3)O(4)·C(10)H(8)N(2)O(2)·H(2)O, are twisted by 14.0 (2)°. The –CO(2)H substituents of the 5-amino-2,4,6-triiodo­isophthalic acid are twisted by 83.0 (2) and 86.5 (2)° out of the plane of the aromatic ring. In the crystal, the three components are linked by O—H⋯O hydrogen bonds into a three-dimensional network. An N—H⋯O inter­action also occurs. One of the amino H atom is not involved in hydrogen bonding.
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spelling pubmed-30997512011-07-13 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1) Zhang, Kou-Lin Zhang, Jin-Bo Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers The aromatic rings of the N,N′-dioxide molecule in the title compound, C(8)H(4)NI(3)O(4)·C(10)H(8)N(2)O(2)·H(2)O, are twisted by 14.0 (2)°. The –CO(2)H substituents of the 5-amino-2,4,6-triiodo­isophthalic acid are twisted by 83.0 (2) and 86.5 (2)° out of the plane of the aromatic ring. In the crystal, the three components are linked by O—H⋯O hydrogen bonds into a three-dimensional network. An N—H⋯O inter­action also occurs. One of the amino H atom is not involved in hydrogen bonding. International Union of Crystallography 2011-03-05 /pmc/articles/PMC3099751/ /pubmed/21754083 http://dx.doi.org/10.1107/S1600536811007276 Text en © Zhang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Kou-Lin
Zhang, Jin-Bo
Ng, Seik Weng
5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title_full 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title_fullStr 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title_full_unstemmed 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title_short 5-Amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine N,N′-dioxide–water (1/1/1)
title_sort 5-amino-2,4,6-triiodo­isophthalic acid–4,4′-bipyridine n,n′-dioxide–water (1/1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099751/
https://www.ncbi.nlm.nih.gov/pubmed/21754083
http://dx.doi.org/10.1107/S1600536811007276
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