N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide

In the crystal of the title compound, C(20)H(22)Cl(2)N(2)O(6)S(2), the asymmetric unit comprises half of a mol­ecule, the remaining portion is generated via an inversion centre. The conformation of the N—H and C=O bonds in the SO(2)–NH–C(O)–C segment is anti. The mol­ecule is bent at the S atom with...

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Detalles Bibliográficos
Autores principales: Rodrigues, Vinola Z., Foro, Sabine, Gowda, B. Thimme
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099798/
https://www.ncbi.nlm.nih.gov/pubmed/21754161
http://dx.doi.org/10.1107/S1600536811009196
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author Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
author_facet Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
author_sort Rodrigues, Vinola Z.
collection PubMed
description In the crystal of the title compound, C(20)H(22)Cl(2)N(2)O(6)S(2), the asymmetric unit comprises half of a mol­ecule, the remaining portion is generated via an inversion centre. The conformation of the N—H and C=O bonds in the SO(2)–NH–C(O)–C segment is anti. The mol­ecule is bent at the S atom with the C–SO(2)–NH–C(O) torsion angle being 68.16 (19)°. The dihedral angle between the plane of the benzene ring and the SO(2)–NH–C(O)–C segment is 77.5 (1)°. Hydrogen bonds of the type N—H⋯O(C) link mol­ecules into supra­molecular chains along the b axis.
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spelling pubmed-30997982011-07-13 N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide Rodrigues, Vinola Z. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal of the title compound, C(20)H(22)Cl(2)N(2)O(6)S(2), the asymmetric unit comprises half of a mol­ecule, the remaining portion is generated via an inversion centre. The conformation of the N—H and C=O bonds in the SO(2)–NH–C(O)–C segment is anti. The mol­ecule is bent at the S atom with the C–SO(2)–NH–C(O) torsion angle being 68.16 (19)°. The dihedral angle between the plane of the benzene ring and the SO(2)–NH–C(O)–C segment is 77.5 (1)°. Hydrogen bonds of the type N—H⋯O(C) link mol­ecules into supra­molecular chains along the b axis. International Union of Crystallography 2011-03-15 /pmc/articles/PMC3099798/ /pubmed/21754161 http://dx.doi.org/10.1107/S1600536811009196 Text en © Rodrigues et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title_full N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title_fullStr N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title_full_unstemmed N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title_short N,N′-Bis(2-chloro­phenyl­sulfon­yl)suberamide
title_sort n,n′-bis(2-chloro­phenyl­sulfon­yl)suberamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099798/
https://www.ncbi.nlm.nih.gov/pubmed/21754161
http://dx.doi.org/10.1107/S1600536811009196
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