2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate

In the crystal structure of the title compound, C(4)H(12)N(+)·C(9)H(3)Br(4)O(4) (−)·CH(4)O, inter­molecular O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds link the components into columns stacked along the b axis. Between the columns, short Br⋯O contacts [3.122 (4) Å] and C—H⋯O hydrogen bonds are observed....

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Detalles Bibliográficos
Autor principal: Li, Jian
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099836/
https://www.ncbi.nlm.nih.gov/pubmed/21754148
http://dx.doi.org/10.1107/S1600536811008518
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author Li, Jian
author_facet Li, Jian
author_sort Li, Jian
collection PubMed
description In the crystal structure of the title compound, C(4)H(12)N(+)·C(9)H(3)Br(4)O(4) (−)·CH(4)O, inter­molecular O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds link the components into columns stacked along the b axis. Between the columns, short Br⋯O contacts [3.122 (4) Å] and C—H⋯O hydrogen bonds are observed.
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spelling pubmed-30998362011-07-13 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate Li, Jian Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(4)H(12)N(+)·C(9)H(3)Br(4)O(4) (−)·CH(4)O, inter­molecular O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds link the components into columns stacked along the b axis. Between the columns, short Br⋯O contacts [3.122 (4) Å] and C—H⋯O hydrogen bonds are observed. International Union of Crystallography 2011-03-12 /pmc/articles/PMC3099836/ /pubmed/21754148 http://dx.doi.org/10.1107/S1600536811008518 Text en © Jian Li 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Jian
2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title_full 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title_fullStr 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title_full_unstemmed 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title_short 2-Methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
title_sort 2-methyl­propan-2-aminium 3,4,5,6-tetra­bromo-2-(meth­oxy­carbon­yl)benzoate methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099836/
https://www.ncbi.nlm.nih.gov/pubmed/21754148
http://dx.doi.org/10.1107/S1600536811008518
work_keys_str_mv AT lijian 2methylpropan2aminium3456tetrabromo2methoxycarbonylbenzoatemethanolmonosolvate

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