Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]

In the anion of the title salt, C(6)H(18)N(2) (2+)·2C(9)H(3)Cl(4)O(4) (−), the meth­oxy­carbonyl and carboxyl groups are aligned at dihedral angles of 71.0 (3) and 100.9 (3)°, respectively, with the aromatic ring. The asymmetric unit contains half a cation and one anion. In the crystal, inter­molecu...

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Autor principal: Li, Jian
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099857/
https://www.ncbi.nlm.nih.gov/pubmed/21754175
http://dx.doi.org/10.1107/S1600536811008506
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author Li, Jian
author_facet Li, Jian
author_sort Li, Jian
collection PubMed
description In the anion of the title salt, C(6)H(18)N(2) (2+)·2C(9)H(3)Cl(4)O(4) (−), the meth­oxy­carbonyl and carboxyl groups are aligned at dihedral angles of 71.0 (3) and 100.9 (3)°, respectively, with the aromatic ring. The asymmetric unit contains half a cation and one anion. In the crystal, inter­molecular N—H⋯O, C—H⋯Cl and C—H⋯O hydrogen bonds link the components into a three-dimensional network.
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spelling pubmed-30998572011-07-13 Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate] Li, Jian Acta Crystallogr Sect E Struct Rep Online Organic Papers In the anion of the title salt, C(6)H(18)N(2) (2+)·2C(9)H(3)Cl(4)O(4) (−), the meth­oxy­carbonyl and carboxyl groups are aligned at dihedral angles of 71.0 (3) and 100.9 (3)°, respectively, with the aromatic ring. The asymmetric unit contains half a cation and one anion. In the crystal, inter­molecular N—H⋯O, C—H⋯Cl and C—H⋯O hydrogen bonds link the components into a three-dimensional network. International Union of Crystallography 2011-03-15 /pmc/articles/PMC3099857/ /pubmed/21754175 http://dx.doi.org/10.1107/S1600536811008506 Text en © Jian Li 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Jian
Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title_full Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title_fullStr Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title_full_unstemmed Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title_short Hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
title_sort hexane-1,6-diaminium bis­[3,4,5,6-tetra­chloro-2-(meth­oxy­carbon­yl)benzoate]
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099857/
https://www.ncbi.nlm.nih.gov/pubmed/21754175
http://dx.doi.org/10.1107/S1600536811008506
work_keys_str_mv AT lijian hexane16diaminiumbis3456tetrachloro2methoxycarbonylbenzoate

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