rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate

The title compound, C(11)H(14)N(2)O(5), was synthesized by condensation of (RS)-2-amino­succinic acid dimethyl ester with 2-trichloro­acetyl­pyrrole at room temperature. The amide group is twisted by 7.4 (1)° from the plane of the pyrrole ring. In the crystal, mol­ecules are linked by inter­molecula...

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Detalles Bibliográficos
Autores principales: Zheng, Le, Hu, Fang, Zeng, Xiang Chao, Li, Kai Ping
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099858/
https://www.ncbi.nlm.nih.gov/pubmed/21754049
http://dx.doi.org/10.1107/S1600536811007148
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author Zheng, Le
Hu, Fang
Zeng, Xiang Chao
Li, Kai Ping
author_facet Zheng, Le
Hu, Fang
Zeng, Xiang Chao
Li, Kai Ping
author_sort Zheng, Le
collection PubMed
description The title compound, C(11)H(14)N(2)O(5), was synthesized by condensation of (RS)-2-amino­succinic acid dimethyl ester with 2-trichloro­acetyl­pyrrole at room temperature. The amide group is twisted by 7.4 (1)° from the plane of the pyrrole ring. In the crystal, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds into chains extending along the c axis.
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spelling pubmed-30998582011-07-13 rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate Zheng, Le Hu, Fang Zeng, Xiang Chao Li, Kai Ping Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(14)N(2)O(5), was synthesized by condensation of (RS)-2-amino­succinic acid dimethyl ester with 2-trichloro­acetyl­pyrrole at room temperature. The amide group is twisted by 7.4 (1)° from the plane of the pyrrole ring. In the crystal, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds into chains extending along the c axis. International Union of Crystallography 2011-03-02 /pmc/articles/PMC3099858/ /pubmed/21754049 http://dx.doi.org/10.1107/S1600536811007148 Text en © Zheng et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zheng, Le
Hu, Fang
Zeng, Xiang Chao
Li, Kai Ping
rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title_full rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title_fullStr rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title_full_unstemmed rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title_short rac-Dimethyl 2-(1H-pyrrole-2-carboxamido)­butane­dioate
title_sort rac-dimethyl 2-(1h-pyrrole-2-carboxamido)­butane­dioate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099858/
https://www.ncbi.nlm.nih.gov/pubmed/21754049
http://dx.doi.org/10.1107/S1600536811007148
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AT hufang racdimethyl21hpyrrole2carboxamidobutanedioate
AT zengxiangchao racdimethyl21hpyrrole2carboxamidobutanedioate
AT likaiping racdimethyl21hpyrrole2carboxamidobutanedioate

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