4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide

There are two independent mol­ecules in the asymmetric unit of the title compound, C(22)H(21)N(3)O(4)S. The central benzene ring makes dihedral angles of 74.28 (6) and 68.84 (6)° with the pyridine and 3,5-dimeth­oxy­phenyl rings, respectively, in one molecule [86.66 (6) and 81.14 (6)° respectively,...

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Detalles Bibliográficos
Autores principales: Huang, Ting-Ting, Meng, Na-Na, Qing, Xiao-Yu, Yu, Luo-Ting
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099903/
https://www.ncbi.nlm.nih.gov/pubmed/21754137
http://dx.doi.org/10.1107/S1600536811006490
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author Huang, Ting-Ting
Meng, Na-Na
Qing, Xiao-Yu
Yu, Luo-Ting
author_facet Huang, Ting-Ting
Meng, Na-Na
Qing, Xiao-Yu
Yu, Luo-Ting
author_sort Huang, Ting-Ting
collection PubMed
description There are two independent mol­ecules in the asymmetric unit of the title compound, C(22)H(21)N(3)O(4)S. The central benzene ring makes dihedral angles of 74.28 (6) and 68.84 (6)° with the pyridine and 3,5-dimeth­oxy­phenyl rings, respectively, in one molecule [86.66 (6) and 81.14 (6)° respectively, in the other]. Each of the mol­ecules forms a centrosymmetric dimer with another mol­ecule via pairs of inter­molecular N—H⋯O hydrogen bonds. These hydrogen bonds connect the N—H groups and the O atoms of the carbonyl groups next to the 3,5-dimeth­oxy­phenyl rings. Additional inter­molecular N—H⋯O inter­actions link the dimers in the crystal structure.
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spelling pubmed-30999032011-07-13 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide Huang, Ting-Ting Meng, Na-Na Qing, Xiao-Yu Yu, Luo-Ting Acta Crystallogr Sect E Struct Rep Online Organic Papers There are two independent mol­ecules in the asymmetric unit of the title compound, C(22)H(21)N(3)O(4)S. The central benzene ring makes dihedral angles of 74.28 (6) and 68.84 (6)° with the pyridine and 3,5-dimeth­oxy­phenyl rings, respectively, in one molecule [86.66 (6) and 81.14 (6)° respectively, in the other]. Each of the mol­ecules forms a centrosymmetric dimer with another mol­ecule via pairs of inter­molecular N—H⋯O hydrogen bonds. These hydrogen bonds connect the N—H groups and the O atoms of the carbonyl groups next to the 3,5-dimeth­oxy­phenyl rings. Additional inter­molecular N—H⋯O inter­actions link the dimers in the crystal structure. International Union of Crystallography 2011-03-12 /pmc/articles/PMC3099903/ /pubmed/21754137 http://dx.doi.org/10.1107/S1600536811006490 Text en © Huang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Huang, Ting-Ting
Meng, Na-Na
Qing, Xiao-Yu
Yu, Luo-Ting
4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title_full 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title_fullStr 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title_full_unstemmed 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title_short 4-{[4-(3,5-Dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-N-methyl­pyridine-2-carboxamide
title_sort 4-{[4-(3,5-dimeth­oxy­benzamido)­phen­yl]sulfan­yl}-n-methyl­pyridine-2-carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099903/
https://www.ncbi.nlm.nih.gov/pubmed/21754137
http://dx.doi.org/10.1107/S1600536811006490
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AT qingxiaoyu 4435dimethoxybenzamidophenylsulfanylnmethylpyridine2carboxamide
AT yuluoting 4435dimethoxybenzamidophenylsulfanylnmethylpyridine2carboxamide

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