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(E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate
The molecule of the title Schiff base compound, C(15)H(14)N(2)O(5), was obtained from a condensation reaction of 4-acetoxy-3-methoxybenzaldehyde and 2-furylcarbonylhydrazide. In the molecule, the furyl ring makes a dihedral angle of 14.63 (10)° with the benzene ring. In the crystal, intermol...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2011
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099912/ https://www.ncbi.nlm.nih.gov/pubmed/21754157 http://dx.doi.org/10.1107/S1600536811008932 |
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author | Xu, Jun Yue, Xiao-yu |
author_facet | Xu, Jun Yue, Xiao-yu |
author_sort | Xu, Jun |
collection | PubMed |
description | The molecule of the title Schiff base compound, C(15)H(14)N(2)O(5), was obtained from a condensation reaction of 4-acetoxy-3-methoxybenzaldehyde and 2-furylcarbonylhydrazide. In the molecule, the furyl ring makes a dihedral angle of 14.63 (10)° with the benzene ring. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the b axis. Futhermore, weak C—H⋯O interactions connect the chains, forming corrugated layers parallel to (001). The dihedral angle between the rings is 14.63 (10)°. |
format | Text |
id | pubmed-3099912 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30999122011-07-13 (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate Xu, Jun Yue, Xiao-yu Acta Crystallogr Sect E Struct Rep Online Organic Papers The molecule of the title Schiff base compound, C(15)H(14)N(2)O(5), was obtained from a condensation reaction of 4-acetoxy-3-methoxybenzaldehyde and 2-furylcarbonylhydrazide. In the molecule, the furyl ring makes a dihedral angle of 14.63 (10)° with the benzene ring. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the b axis. Futhermore, weak C—H⋯O interactions connect the chains, forming corrugated layers parallel to (001). The dihedral angle between the rings is 14.63 (10)°. International Union of Crystallography 2011-03-15 /pmc/articles/PMC3099912/ /pubmed/21754157 http://dx.doi.org/10.1107/S1600536811008932 Text en © Xu and Yue 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Xu, Jun Yue, Xiao-yu (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title | (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title_full | (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title_fullStr | (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title_full_unstemmed | (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title_short | (E)-4-{[2-(2-Furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
title_sort | (e)-4-{[2-(2-furylcarbonyl)hydrazinylidene]methyl}-2-methoxyphenyl acetate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3099912/ https://www.ncbi.nlm.nih.gov/pubmed/21754157 http://dx.doi.org/10.1107/S1600536811008932 |
work_keys_str_mv | AT xujun e422furylcarbonylhydrazinylidenemethyl2methoxyphenylacetate AT yuexiaoyu e422furylcarbonylhydrazinylidenemethyl2methoxyphenylacetate |