12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]

The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R (p))-4-bromo-12-hy­droxy[2.2]paracyclo­phane and oxydiethane-2,1-diyl bis­(4-methyl­benzene­sulfonate). The crystal packing exhibits a short O⋯Br inter­action [Br⋯O = 3.185 (3) Å] and a weak inter­molecular C—H⋯O contact....

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Detalles Bibliográficos
Autores principales: Hong, Bing, Ma, Yudao, Duan, Wenzeng, He, Fuyan, Zhao, Lei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3100051/
https://www.ncbi.nlm.nih.gov/pubmed/21754216
http://dx.doi.org/10.1107/S1600536811010051
Descripción
Sumario:The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R (p))-4-bromo-12-hy­droxy[2.2]paracyclo­phane and oxydiethane-2,1-diyl bis­(4-methyl­benzene­sulfonate). The crystal packing exhibits a short O⋯Br inter­action [Br⋯O = 3.185 (3) Å] and a weak inter­molecular C—H⋯O contact.

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