12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]

The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R (p))-4-bromo-12-hy­droxy[2.2]paracyclo­phane and oxydiethane-2,1-diyl bis­(4-methyl­benzene­sulfonate). The crystal packing exhibits a short O⋯Br inter­action [Br⋯O = 3.185 (3) Å] and a weak inter­molecular C—H⋯O contact....

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Detalles Bibliográficos
Autores principales: Hong, Bing, Ma, Yudao, Duan, Wenzeng, He, Fuyan, Zhao, Lei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3100051/
https://www.ncbi.nlm.nih.gov/pubmed/21754216
http://dx.doi.org/10.1107/S1600536811010051
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author Hong, Bing
Ma, Yudao
Duan, Wenzeng
He, Fuyan
Zhao, Lei
author_facet Hong, Bing
Ma, Yudao
Duan, Wenzeng
He, Fuyan
Zhao, Lei
author_sort Hong, Bing
collection PubMed
description The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R (p))-4-bromo-12-hy­droxy[2.2]paracyclo­phane and oxydiethane-2,1-diyl bis­(4-methyl­benzene­sulfonate). The crystal packing exhibits a short O⋯Br inter­action [Br⋯O = 3.185 (3) Å] and a weak inter­molecular C—H⋯O contact.
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spelling pubmed-31000512011-07-13 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane] Hong, Bing Ma, Yudao Duan, Wenzeng He, Fuyan Zhao, Lei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R (p))-4-bromo-12-hy­droxy[2.2]paracyclo­phane and oxydiethane-2,1-diyl bis­(4-methyl­benzene­sulfonate). The crystal packing exhibits a short O⋯Br inter­action [Br⋯O = 3.185 (3) Å] and a weak inter­molecular C—H⋯O contact. International Union of Crystallography 2011-03-23 /pmc/articles/PMC3100051/ /pubmed/21754216 http://dx.doi.org/10.1107/S1600536811010051 Text en © Hong et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hong, Bing
Ma, Yudao
Duan, Wenzeng
He, Fuyan
Zhao, Lei
12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title_full 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title_fullStr 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title_full_unstemmed 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title_short 12,12′-[2,2′-Oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(R (p))-4-bromo­[2.2]paracyclo­phane]
title_sort 12,12′-[2,2′-oxybis(ethane-2,1-di­yl)bis­(­oxy)]bis­[(r (p))-4-bromo­[2.2]paracyclo­phane]
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3100051/
https://www.ncbi.nlm.nih.gov/pubmed/21754216
http://dx.doi.org/10.1107/S1600536811010051
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AT mayudao 121222oxybisethane21diylbisoxybisrp4bromo22paracyclophane
AT duanwenzeng 121222oxybisethane21diylbisoxybisrp4bromo22paracyclophane
AT hefuyan 121222oxybisethane21diylbisoxybisrp4bromo22paracyclophane
AT zhaolei 121222oxybisethane21diylbisoxybisrp4bromo22paracyclophane

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