(2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate

The title compound, C(24)H(30)N(2)O(4), was obtained by the reaction of (2R,6S)-4-(tert-but­oxy­carbon­yl)-6-methyl­morpho­line-2-carb­oxy­lic acid with diphenyl­methanamine in dimethyl­formamide solution. The morpholine ring is in a chair conformation. In the crystal, weak inter­molecular C—H⋯O hyd...

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Detalles Bibliográficos
Autores principales: Wang, Haiyang, Xia, Guangxin, Liu, Xuejun, Shen, Jingkang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120296/
https://www.ncbi.nlm.nih.gov/pubmed/21754815
http://dx.doi.org/10.1107/S1600536811017764
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author Wang, Haiyang
Xia, Guangxin
Liu, Xuejun
Shen, Jingkang
author_facet Wang, Haiyang
Xia, Guangxin
Liu, Xuejun
Shen, Jingkang
author_sort Wang, Haiyang
collection PubMed
description The title compound, C(24)H(30)N(2)O(4), was obtained by the reaction of (2R,6S)-4-(tert-but­oxy­carbon­yl)-6-methyl­morpho­line-2-carb­oxy­lic acid with diphenyl­methanamine in dimethyl­formamide solution. The morpholine ring is in a chair conformation. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link mol­ecules into chains along the b axis.
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spelling pubmed-31202962011-07-13 (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate Wang, Haiyang Xia, Guangxin Liu, Xuejun Shen, Jingkang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(24)H(30)N(2)O(4), was obtained by the reaction of (2R,6S)-4-(tert-but­oxy­carbon­yl)-6-methyl­morpho­line-2-carb­oxy­lic acid with diphenyl­methanamine in dimethyl­formamide solution. The morpholine ring is in a chair conformation. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link mol­ecules into chains along the b axis. International Union of Crystallography 2011-05-20 /pmc/articles/PMC3120296/ /pubmed/21754815 http://dx.doi.org/10.1107/S1600536811017764 Text en © Wang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Haiyang
Xia, Guangxin
Liu, Xuejun
Shen, Jingkang
(2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title_full (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title_fullStr (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title_full_unstemmed (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title_short (2R,6S)-tert-Butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
title_sort (2r,6s)-tert-butyl 2-(benzhydryl­carbamo­yl)-6-methyl­morpholine-4-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120296/
https://www.ncbi.nlm.nih.gov/pubmed/21754815
http://dx.doi.org/10.1107/S1600536811017764
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AT liuxuejun 2r6stertbutyl2benzhydrylcarbamoyl6methylmorpholine4carboxylate
AT shenjingkang 2r6stertbutyl2benzhydrylcarbamoyl6methylmorpholine4carboxylate

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