N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate

In the title compound, C(12)H(10)ClN(5)·CH(3)OH, the indazole ring system and the pyrimidine ring make a dihedral angle of 23.86 (4)°. In the crystal, the components are linked by N—H⋯O and O—H⋯N hydrogen bonds into chains propagated in [010]. Inter­molecular π–π inter­actions [centroid–centroid dis...

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Autores principales: Pang, Xiang-Chuan, Deng, Xin-Hua, Sun, Yuan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120303/
https://www.ncbi.nlm.nih.gov/pubmed/21754810
http://dx.doi.org/10.1107/S1600536811017831
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author Pang, Xiang-Chuan
Deng, Xin-Hua
Sun, Yuan
author_facet Pang, Xiang-Chuan
Deng, Xin-Hua
Sun, Yuan
author_sort Pang, Xiang-Chuan
collection PubMed
description In the title compound, C(12)H(10)ClN(5)·CH(3)OH, the indazole ring system and the pyrimidine ring make a dihedral angle of 23.86 (4)°. In the crystal, the components are linked by N—H⋯O and O—H⋯N hydrogen bonds into chains propagated in [010]. Inter­molecular π–π inter­actions [centroid–centroid distances = 3.6404 (9), 3.6725 (9) and 3.4566 (9) Å] between the rings of neighbouring chains also stabilize the crystal packing.
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spelling pubmed-31203032011-07-13 N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate Pang, Xiang-Chuan Deng, Xin-Hua Sun, Yuan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(12)H(10)ClN(5)·CH(3)OH, the indazole ring system and the pyrimidine ring make a dihedral angle of 23.86 (4)°. In the crystal, the components are linked by N—H⋯O and O—H⋯N hydrogen bonds into chains propagated in [010]. Inter­molecular π–π inter­actions [centroid–centroid distances = 3.6404 (9), 3.6725 (9) and 3.4566 (9) Å] between the rings of neighbouring chains also stabilize the crystal packing. International Union of Crystallography 2011-05-14 /pmc/articles/PMC3120303/ /pubmed/21754810 http://dx.doi.org/10.1107/S1600536811017831 Text en © Pang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pang, Xiang-Chuan
Deng, Xin-Hua
Sun, Yuan
N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title_full N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title_fullStr N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title_full_unstemmed N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title_short N-(2-Chloro­pyrimidin-4-yl)-2-methyl-2H-indazol-6-amine methanol monosolvate
title_sort n-(2-chloro­pyrimidin-4-yl)-2-methyl-2h-indazol-6-amine methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120303/
https://www.ncbi.nlm.nih.gov/pubmed/21754810
http://dx.doi.org/10.1107/S1600536811017831
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