N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate

In the title hydrate, C(17)H(18)N(2)O(2)·H(2)O, the dihedral angles formed by the aromatic rings of the benzene and methyl­benzene groups with the mean planes of the attached NH—C(O)—CH(2) fragments are 12.6 (4) and 23.3 (3)°, respectively, while that between the two aromatic rings is 73.7 (2)°. In...

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Detalles Bibliográficos
Autores principales: Saraswathi, B. S., Foro, Sabine, Gowda, B. Thimme
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120322/
https://www.ncbi.nlm.nih.gov/pubmed/21754863
http://dx.doi.org/10.1107/S1600536811018915
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author Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
author_facet Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
author_sort Saraswathi, B. S.
collection PubMed
description In the title hydrate, C(17)H(18)N(2)O(2)·H(2)O, the dihedral angles formed by the aromatic rings of the benzene and methyl­benzene groups with the mean planes of the attached NH—C(O)—CH(2) fragments are 12.6 (4) and 23.3 (3)°, respectively, while that between the two aromatic rings is 73.7 (2)°. In the crystal, the water mol­ecule accepts two and makes two hydrogen bonds. The mol­ecules are packed into layers parallel to (101) by O—H⋯O and N—H⋯O hydrogen-bonding inter­actions.
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spelling pubmed-31203222011-07-13 N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title hydrate, C(17)H(18)N(2)O(2)·H(2)O, the dihedral angles formed by the aromatic rings of the benzene and methyl­benzene groups with the mean planes of the attached NH—C(O)—CH(2) fragments are 12.6 (4) and 23.3 (3)°, respectively, while that between the two aromatic rings is 73.7 (2)°. In the crystal, the water mol­ecule accepts two and makes two hydrogen bonds. The mol­ecules are packed into layers parallel to (101) by O—H⋯O and N—H⋯O hydrogen-bonding inter­actions. International Union of Crystallography 2011-05-25 /pmc/articles/PMC3120322/ /pubmed/21754863 http://dx.doi.org/10.1107/S1600536811018915 Text en © Saraswathi et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title_full N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title_fullStr N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title_full_unstemmed N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title_short N-(4-Methyl­phen­yl)-N′-phenyl­butane­diamide monohydrate
title_sort n-(4-methyl­phen­yl)-n′-phenyl­butane­diamide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120322/
https://www.ncbi.nlm.nih.gov/pubmed/21754863
http://dx.doi.org/10.1107/S1600536811018915
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