5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione

The title compound, C(15)H(16)O(4), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 3,4-dimethyl­benzaldehyde in ethanol. The 1,3-dioxane ring exhibits an envelope conformation. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O hydrogen bonds, forming chains...

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Detalles Bibliográficos
Autor principal: Zeng, Wu-Lan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120337/
https://www.ncbi.nlm.nih.gov/pubmed/21754745
http://dx.doi.org/10.1107/S1600536811016497
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author Zeng, Wu-Lan
author_facet Zeng, Wu-Lan
author_sort Zeng, Wu-Lan
collection PubMed
description The title compound, C(15)H(16)O(4), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 3,4-dimethyl­benzaldehyde in ethanol. The 1,3-dioxane ring exhibits an envelope conformation. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O hydrogen bonds, forming chains parallel to the b axis.
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spelling pubmed-31203372011-07-13 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione Zeng, Wu-Lan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(16)O(4), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 3,4-dimethyl­benzaldehyde in ethanol. The 1,3-dioxane ring exhibits an envelope conformation. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O hydrogen bonds, forming chains parallel to the b axis. International Union of Crystallography 2011-05-07 /pmc/articles/PMC3120337/ /pubmed/21754745 http://dx.doi.org/10.1107/S1600536811016497 Text en © Wu-Lan Zeng 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zeng, Wu-Lan
5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title_full 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title_fullStr 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title_full_unstemmed 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title_short 5-(3,4-Dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
title_sort 5-(3,4-dimethyl­benzyl­idene)-2,2-dimethyl-1,3-dioxane-4,6-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120337/
https://www.ncbi.nlm.nih.gov/pubmed/21754745
http://dx.doi.org/10.1107/S1600536811016497
work_keys_str_mv AT zengwulan 534dimethylbenzylidene22dimethyl13dioxane46dione

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