3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne

In the title compound, C(21)H(22)N(2)O(8), both of the nonplanar six-membered heterocycles adopt chair conformations. The dihedral angle between the terminal benzene rings is 58.22 (11)°. Weak inter­molecular C—H⋯O inter­actions are observed in the crystal structure.

Detalles Bibliográficos
Autores principales: Sun, Xiaoqiang, Yu, Bin, Zhang, Xiuqin, Chao, Xuqiang, Chen, Qiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120352/
https://www.ncbi.nlm.nih.gov/pubmed/21754717
http://dx.doi.org/10.1107/S1600536811015017
_version_ 1782206659825762304
author Sun, Xiaoqiang
Yu, Bin
Zhang, Xiuqin
Chao, Xuqiang
Chen, Qiang
author_facet Sun, Xiaoqiang
Yu, Bin
Zhang, Xiuqin
Chao, Xuqiang
Chen, Qiang
author_sort Sun, Xiaoqiang
collection PubMed
description In the title compound, C(21)H(22)N(2)O(8), both of the nonplanar six-membered heterocycles adopt chair conformations. The dihedral angle between the terminal benzene rings is 58.22 (11)°. Weak inter­molecular C—H⋯O inter­actions are observed in the crystal structure.
format Online
Article
Text
id pubmed-3120352
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-31203522011-07-13 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne Sun, Xiaoqiang Yu, Bin Zhang, Xiuqin Chao, Xuqiang Chen, Qiang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(21)H(22)N(2)O(8), both of the nonplanar six-membered heterocycles adopt chair conformations. The dihedral angle between the terminal benzene rings is 58.22 (11)°. Weak inter­molecular C—H⋯O inter­actions are observed in the crystal structure. International Union of Crystallography 2011-05-07 /pmc/articles/PMC3120352/ /pubmed/21754717 http://dx.doi.org/10.1107/S1600536811015017 Text en © Sun et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sun, Xiaoqiang
Yu, Bin
Zhang, Xiuqin
Chao, Xuqiang
Chen, Qiang
3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title_full 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title_fullStr 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title_full_unstemmed 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title_short 3,9-Dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
title_sort 3,9-dimethyl-3,9-bis­(4-nitro­phen­yl)-2,4,8,10-tetra­oxaspiro­[5.5]undeca­ne
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120352/
https://www.ncbi.nlm.nih.gov/pubmed/21754717
http://dx.doi.org/10.1107/S1600536811015017
work_keys_str_mv AT sunxiaoqiang 39dimethyl39bis4nitrophenyl24810tetraoxaspiro55undecane
AT yubin 39dimethyl39bis4nitrophenyl24810tetraoxaspiro55undecane
AT zhangxiuqin 39dimethyl39bis4nitrophenyl24810tetraoxaspiro55undecane
AT chaoxuqiang 39dimethyl39bis4nitrophenyl24810tetraoxaspiro55undecane
AT chenqiang 39dimethyl39bis4nitrophenyl24810tetraoxaspiro55undecane

Ejemplares similares