{2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron

The title compound, C(22)H(22)BNO(3), was unintentionally obtained from salicyl­aldehyde benzyl­amine and sodium borohydride. The B—O bond lengths lie in the range 1.425 (2)–1.463 (2) Å, and B—N = 1.641 (2) Å. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains...

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Detalles Bibliográficos
Autores principales: Geng, Yanxia, Wu, Wangsuo
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120563/
https://www.ncbi.nlm.nih.gov/pubmed/21754770
http://dx.doi.org/10.1107/S1600536811016990
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author Geng, Yanxia
Wu, Wangsuo
author_facet Geng, Yanxia
Wu, Wangsuo
author_sort Geng, Yanxia
collection PubMed
description The title compound, C(22)H(22)BNO(3), was unintentionally obtained from salicyl­aldehyde benzyl­amine and sodium borohydride. The B—O bond lengths lie in the range 1.425 (2)–1.463 (2) Å, and B—N = 1.641 (2) Å. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains in the [010] direction.
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spelling pubmed-31205632011-07-13 {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron Geng, Yanxia Wu, Wangsuo Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(22)H(22)BNO(3), was unintentionally obtained from salicyl­aldehyde benzyl­amine and sodium borohydride. The B—O bond lengths lie in the range 1.425 (2)–1.463 (2) Å, and B—N = 1.641 (2) Å. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains in the [010] direction. International Union of Crystallography 2011-05-11 /pmc/articles/PMC3120563/ /pubmed/21754770 http://dx.doi.org/10.1107/S1600536811016990 Text en © Geng and Wu 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Geng, Yanxia
Wu, Wangsuo
{2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title_full {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title_fullStr {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title_full_unstemmed {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title_short {2,2′-[(Benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
title_sort {2,2′-[(benzyl­aza­nedi­yl)dimethylene]diphenolato}(methano­lato)boron
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3120563/
https://www.ncbi.nlm.nih.gov/pubmed/21754770
http://dx.doi.org/10.1107/S1600536811016990
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AT wuwangsuo 22benzylazanediyldimethylenediphenolatomethanolatoboron

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