Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method

The aim of the current work is the synthesis and characterization of metallic Zr nanoparticles. The preparation is carried out by using the RAPET method (Reaction under Autogenic Pressure at Elevated Temperatures) developed in our lab. The RAPET reaction of commercial ZrO(2) with Mg powder was carri...

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Autores principales: Eshed, Michal, Pol, Swati, Gedanken, Aharon, Balasubramanian, Mahalingam
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2011
Materias:
Full Research Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3148038/
https://www.ncbi.nlm.nih.gov/pubmed/21977431
http://dx.doi.org/10.3762/bjnano.2.23
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author Eshed, Michal
Pol, Swati
Gedanken, Aharon
Balasubramanian, Mahalingam
author_facet Eshed, Michal
Pol, Swati
Gedanken, Aharon
Balasubramanian, Mahalingam
author_sort Eshed, Michal
collection PubMed
description The aim of the current work is the synthesis and characterization of metallic Zr nanoparticles. The preparation is carried out by using the RAPET method (Reaction under Autogenic Pressure at Elevated Temperatures) developed in our lab. The RAPET reaction of commercial ZrO(2) with Mg powder was carried out in a closed stainless steel cell, at 750 °C. On completion of the reaction, the additionally formed MgO is removed by treatment with acid. The characterization of the product was performed by XRD, X-ray absorption spectroscopy, SEM, TEM and elemental analysis. The XRD pattern reveals that the product is composed of pure metallic zirconium, without any traces of the MgO by-product.
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spelling pubmed-31480382011-10-05 Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method Eshed, Michal Pol, Swati Gedanken, Aharon Balasubramanian, Mahalingam Beilstein J Nanotechnol Full Research Paper The aim of the current work is the synthesis and characterization of metallic Zr nanoparticles. The preparation is carried out by using the RAPET method (Reaction under Autogenic Pressure at Elevated Temperatures) developed in our lab. The RAPET reaction of commercial ZrO(2) with Mg powder was carried out in a closed stainless steel cell, at 750 °C. On completion of the reaction, the additionally formed MgO is removed by treatment with acid. The characterization of the product was performed by XRD, X-ray absorption spectroscopy, SEM, TEM and elemental analysis. The XRD pattern reveals that the product is composed of pure metallic zirconium, without any traces of the MgO by-product. Beilstein-Institut 2011-04-06 /pmc/articles/PMC3148038/ /pubmed/21977431 http://dx.doi.org/10.3762/bjnano.2.23 Text en Copyright © 2011, Eshed et al. https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjnano/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms)
spellingShingle Full Research Paper
Eshed, Michal
Pol, Swati
Gedanken, Aharon
Balasubramanian, Mahalingam
Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title_full Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title_fullStr Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title_full_unstemmed Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title_short Zirconium nanoparticles prepared by the reduction of zirconium oxide using the RAPET method
title_sort zirconium nanoparticles prepared by the reduction of zirconium oxide using the rapet method
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3148038/
https://www.ncbi.nlm.nih.gov/pubmed/21977431
http://dx.doi.org/10.3762/bjnano.2.23
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