1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione

In the crystal structure of the title mol­ecule, C(26)H(32)N(2)O(2), the six methyl groups are disordered over two positions, with site-occupancy ratios of 0.665 (8):0.335 (8) and 0.639 (8):0.361 (8). The central pyrimidine ring is almost planar with an r.m.s. deviation of 0.009 Å. The dihedral angl...

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Detalles Bibliográficos
Autores principales: Li, Gong-Chun, Wang, Hong-Sheng, Zhu, Feng-Xiang, Niu, Yu-Jiao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151810/
https://www.ncbi.nlm.nih.gov/pubmed/21837016
http://dx.doi.org/10.1107/S160053681102054X
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author Li, Gong-Chun
Wang, Hong-Sheng
Zhu, Feng-Xiang
Niu, Yu-Jiao
author_facet Li, Gong-Chun
Wang, Hong-Sheng
Zhu, Feng-Xiang
Niu, Yu-Jiao
author_sort Li, Gong-Chun
collection PubMed
description In the crystal structure of the title mol­ecule, C(26)H(32)N(2)O(2), the six methyl groups are disordered over two positions, with site-occupancy ratios of 0.665 (8):0.335 (8) and 0.639 (8):0.361 (8). The central pyrimidine ring is almost planar with an r.m.s. deviation of 0.009 Å. The dihedral angles formed by the two benzene rings with the pyrimidine ring are 70.70 (8) and 88.02 (9)°. The dihedral angle between two benzene rings is 46.67 (10)°.
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spelling pubmed-31518102011-08-11 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione Li, Gong-Chun Wang, Hong-Sheng Zhu, Feng-Xiang Niu, Yu-Jiao Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title mol­ecule, C(26)H(32)N(2)O(2), the six methyl groups are disordered over two positions, with site-occupancy ratios of 0.665 (8):0.335 (8) and 0.639 (8):0.361 (8). The central pyrimidine ring is almost planar with an r.m.s. deviation of 0.009 Å. The dihedral angles formed by the two benzene rings with the pyrimidine ring are 70.70 (8) and 88.02 (9)°. The dihedral angle between two benzene rings is 46.67 (10)°. International Union of Crystallography 2011-06-11 /pmc/articles/PMC3151810/ /pubmed/21837016 http://dx.doi.org/10.1107/S160053681102054X Text en © Li et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Gong-Chun
Wang, Hong-Sheng
Zhu, Feng-Xiang
Niu, Yu-Jiao
1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title_full 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title_fullStr 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title_full_unstemmed 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title_short 1,3-Bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1H,3H)-dione
title_sort 1,3-bis(4-tert-butyl­benz­yl)pyrimidine-2,4(1h,3h)-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151810/
https://www.ncbi.nlm.nih.gov/pubmed/21837016
http://dx.doi.org/10.1107/S160053681102054X
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