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Pimelic acid–urea (1/2)

The asymmetric unit, 2CH(4)N(2)O·C(7)H(12)O(4), of the title cocrystal contains one urea mol­ecule and a half-mol­ecule of pimelic acid; the latter, together with a second urea mol­ecule, are completed by symmetry, with the central atom of the whole pimelic acid moiety placed on a twofold crystallog...

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Detalles Bibliográficos
Autores principales: Xu, Wei, Huang, Wen-xiang, Chen, Hong-yan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151831/
https://www.ncbi.nlm.nih.gov/pubmed/21837168
http://dx.doi.org/10.1107/S1600536811023439
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author Xu, Wei
Huang, Wen-xiang
Chen, Hong-yan
author_facet Xu, Wei
Huang, Wen-xiang
Chen, Hong-yan
author_sort Xu, Wei
collection PubMed
description The asymmetric unit, 2CH(4)N(2)O·C(7)H(12)O(4), of the title cocrystal contains one urea mol­ecule and a half-mol­ecule of pimelic acid; the latter, together with a second urea mol­ecule, are completed by symmetry, with the central atom of the whole pimelic acid moiety placed on a twofold crystallographic axis. The crystal packing is stabilized by O—H⋯O and N—H⋯O hydrogen-bond, generating a chain along [10[Image: see text]]. Additionally, the chains are assembled into a three-dimensional framework via weak N—H⋯O inter­chain inter­actions.
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spelling pubmed-31518312011-08-11 Pimelic acid–urea (1/2) Xu, Wei Huang, Wen-xiang Chen, Hong-yan Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit, 2CH(4)N(2)O·C(7)H(12)O(4), of the title cocrystal contains one urea mol­ecule and a half-mol­ecule of pimelic acid; the latter, together with a second urea mol­ecule, are completed by symmetry, with the central atom of the whole pimelic acid moiety placed on a twofold crystallographic axis. The crystal packing is stabilized by O—H⋯O and N—H⋯O hydrogen-bond, generating a chain along [10[Image: see text]]. Additionally, the chains are assembled into a three-dimensional framework via weak N—H⋯O inter­chain inter­actions. International Union of Crystallography 2011-06-25 /pmc/articles/PMC3151831/ /pubmed/21837168 http://dx.doi.org/10.1107/S1600536811023439 Text en © Xu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xu, Wei
Huang, Wen-xiang
Chen, Hong-yan
Pimelic acid–urea (1/2)
title Pimelic acid–urea (1/2)
title_full Pimelic acid–urea (1/2)
title_fullStr Pimelic acid–urea (1/2)
title_full_unstemmed Pimelic acid–urea (1/2)
title_short Pimelic acid–urea (1/2)
title_sort pimelic acid–urea (1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151831/
https://www.ncbi.nlm.nih.gov/pubmed/21837168
http://dx.doi.org/10.1107/S1600536811023439
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