(S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide

In the crystal structure of the title mol­ecule, C(13)H(18)BrO(4)P, the phospho­nate ring adopts a chair conformation. Mol­ecules are linked by an O—H⋯O hydrogen bond [O⋯O = 2.780 (3) Å] to form chains parallel to the c axis. Two C—H⋯O inter­actions help to stabilize the crystal structure....

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Detalles Bibliográficos
Autores principales: Wang, Chubei, Peng, Hao, He, Hongwu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151866/
https://www.ncbi.nlm.nih.gov/pubmed/21837127
http://dx.doi.org/10.1107/S1600536811020587
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author Wang, Chubei
Peng, Hao
He, Hongwu
author_facet Wang, Chubei
Peng, Hao
He, Hongwu
author_sort Wang, Chubei
collection PubMed
description In the crystal structure of the title mol­ecule, C(13)H(18)BrO(4)P, the phospho­nate ring adopts a chair conformation. Mol­ecules are linked by an O—H⋯O hydrogen bond [O⋯O = 2.780 (3) Å] to form chains parallel to the c axis. Two C—H⋯O inter­actions help to stabilize the crystal structure.
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spelling pubmed-31518662011-08-11 (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide Wang, Chubei Peng, Hao He, Hongwu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title mol­ecule, C(13)H(18)BrO(4)P, the phospho­nate ring adopts a chair conformation. Mol­ecules are linked by an O—H⋯O hydrogen bond [O⋯O = 2.780 (3) Å] to form chains parallel to the c axis. Two C—H⋯O inter­actions help to stabilize the crystal structure. International Union of Crystallography 2011-06-18 /pmc/articles/PMC3151866/ /pubmed/21837127 http://dx.doi.org/10.1107/S1600536811020587 Text en © Wang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Chubei
Peng, Hao
He, Hongwu
(S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title_full (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title_fullStr (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title_full_unstemmed (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title_short (S)-2-[1-(4-Bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
title_sort (s)-2-[1-(4-bromo­phen­yl)-1-hy­droxy­ethyl]-5,5-dimethyl-1,3,2-dioxaphos­phinane 2-oxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151866/
https://www.ncbi.nlm.nih.gov/pubmed/21837127
http://dx.doi.org/10.1107/S1600536811020587
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AT hehongwu s214bromophenyl1hydroxyethyl55dimethyl132dioxaphosphinane2oxide

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