4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid

The title compound, C(15)H(21)NO(4)S, crystallized with two independent mol­ecules in the asymmetric unit in which the dihedral angles between the mean planes of the benzene and cyclo­hexane rings are 78.3 (2) and 67.6 (2)°. The substituents of the cyclo­hexyl rings are in equatorial orientations. I...

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Autores principales: Ashfaq, Muhammad, Iram, Samina, Akkurt, Mehmet, Khan, Islam Ullah, Mustafa, Ghulam, Sharif, Shahzad
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151904/
https://www.ncbi.nlm.nih.gov/pubmed/21836976
http://dx.doi.org/10.1107/S1600536811020083
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author Ashfaq, Muhammad
Iram, Samina
Akkurt, Mehmet
Khan, Islam Ullah
Mustafa, Ghulam
Sharif, Shahzad
author_facet Ashfaq, Muhammad
Iram, Samina
Akkurt, Mehmet
Khan, Islam Ullah
Mustafa, Ghulam
Sharif, Shahzad
author_sort Ashfaq, Muhammad
collection PubMed
description The title compound, C(15)H(21)NO(4)S, crystallized with two independent mol­ecules in the asymmetric unit in which the dihedral angles between the mean planes of the benzene and cyclo­hexane rings are 78.3 (2) and 67.6 (2)°. The substituents of the cyclo­hexyl rings are in equatorial orientations. In the crystal, both mol­ecules form R (2) (2)(6) carb­oxy­lic acid inversion dimers via pairs of O—H⋯O hydrogen bonds. Further N—H⋯O and C—H⋯O inter­actions generate a three-dimensional network.
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spelling pubmed-31519042011-08-11 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid Ashfaq, Muhammad Iram, Samina Akkurt, Mehmet Khan, Islam Ullah Mustafa, Ghulam Sharif, Shahzad Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(21)NO(4)S, crystallized with two independent mol­ecules in the asymmetric unit in which the dihedral angles between the mean planes of the benzene and cyclo­hexane rings are 78.3 (2) and 67.6 (2)°. The substituents of the cyclo­hexyl rings are in equatorial orientations. In the crystal, both mol­ecules form R (2) (2)(6) carb­oxy­lic acid inversion dimers via pairs of O—H⋯O hydrogen bonds. Further N—H⋯O and C—H⋯O inter­actions generate a three-dimensional network. International Union of Crystallography 2011-06-04 /pmc/articles/PMC3151904/ /pubmed/21836976 http://dx.doi.org/10.1107/S1600536811020083 Text en © Ashfaq et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ashfaq, Muhammad
Iram, Samina
Akkurt, Mehmet
Khan, Islam Ullah
Mustafa, Ghulam
Sharif, Shahzad
4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title_full 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title_fullStr 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title_full_unstemmed 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title_short 4-[(4-Methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
title_sort 4-[(4-methyl­benzene­sulfonamido)­meth­yl]cyclo­hexa­necarb­oxy­lic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151904/
https://www.ncbi.nlm.nih.gov/pubmed/21836976
http://dx.doi.org/10.1107/S1600536811020083
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