Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)

In the crystal structure of the title compound, C(4)H(8)N(2)O(4)·C(18)H(15)OP, two triphenyl­phosphine oxide mol­ecules and two dimethyl hydrazine-1,2-dicarboxyl­ate mol­ecules are connected via N—H⋯O hydrogen bonds of moderate strength and are related via a twofold rotational axis. Weak C(ar)—H⋯ O...

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Autores principales: Doboszewski, Bogdan, McGarrah, James, Nazarenko, Alexander Y., da Paixao Soares, Fabio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151943/
https://www.ncbi.nlm.nih.gov/pubmed/21836978
http://dx.doi.org/10.1107/S160053681101991X
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author Doboszewski, Bogdan
McGarrah, James
Nazarenko, Alexander Y.
da Paixao Soares, Fabio
author_facet Doboszewski, Bogdan
McGarrah, James
Nazarenko, Alexander Y.
da Paixao Soares, Fabio
author_sort Doboszewski, Bogdan
collection PubMed
description In the crystal structure of the title compound, C(4)H(8)N(2)O(4)·C(18)H(15)OP, two triphenyl­phosphine oxide mol­ecules and two dimethyl hydrazine-1,2-dicarboxyl­ate mol­ecules are connected via N—H⋯O hydrogen bonds of moderate strength and are related via a twofold rotational axis. Weak C(ar)—H⋯ O contacts strengthen the crystal structure.
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spelling pubmed-31519432011-08-11 Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1) Doboszewski, Bogdan McGarrah, James Nazarenko, Alexander Y. da Paixao Soares, Fabio Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(4)H(8)N(2)O(4)·C(18)H(15)OP, two triphenyl­phosphine oxide mol­ecules and two dimethyl hydrazine-1,2-dicarboxyl­ate mol­ecules are connected via N—H⋯O hydrogen bonds of moderate strength and are related via a twofold rotational axis. Weak C(ar)—H⋯ O contacts strengthen the crystal structure. International Union of Crystallography 2011-06-04 /pmc/articles/PMC3151943/ /pubmed/21836978 http://dx.doi.org/10.1107/S160053681101991X Text en © Doboszewski et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Doboszewski, Bogdan
McGarrah, James
Nazarenko, Alexander Y.
da Paixao Soares, Fabio
Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title_full Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title_fullStr Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title_full_unstemmed Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title_short Dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
title_sort dimethyl hydrazine-1,2-dicarboxyl­ate–triphenyl­phosphine oxide (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151943/
https://www.ncbi.nlm.nih.gov/pubmed/21836978
http://dx.doi.org/10.1107/S160053681101991X
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