(E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate

In the hydrazone molecule of the title compound, C(13)H(9)I(2)N(3)O(2)·CH(3)CN, the aromatic rings form a dihedral angle of 9.4 (3)°. In the crystal structure, inter­molecular I⋯N inter­actions [3.099 (4) Å] link hydrogen-bonded aggregates of the hydrozone and solvent molecules related by translatio...

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Detalles Bibliográficos
Autores principales: Sun, Shan-Shan, Liu, Shi-Yong, Zheng, Ting-Ting, Wang, Xiao-Ling
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151945/
https://www.ncbi.nlm.nih.gov/pubmed/21837030
http://dx.doi.org/10.1107/S1600536811020770
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author Sun, Shan-Shan
Liu, Shi-Yong
Zheng, Ting-Ting
Wang, Xiao-Ling
author_facet Sun, Shan-Shan
Liu, Shi-Yong
Zheng, Ting-Ting
Wang, Xiao-Ling
author_sort Sun, Shan-Shan
collection PubMed
description In the hydrazone molecule of the title compound, C(13)H(9)I(2)N(3)O(2)·CH(3)CN, the aromatic rings form a dihedral angle of 9.4 (3)°. In the crystal structure, inter­molecular I⋯N inter­actions [3.099 (4) Å] link hydrogen-bonded aggregates of the hydrozone and solvent molecules related by translation along the b axis into chains. An intramolecular O—H⋯N hydrogen bond forms an S(6) ring.
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spelling pubmed-31519452011-08-11 (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate Sun, Shan-Shan Liu, Shi-Yong Zheng, Ting-Ting Wang, Xiao-Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers In the hydrazone molecule of the title compound, C(13)H(9)I(2)N(3)O(2)·CH(3)CN, the aromatic rings form a dihedral angle of 9.4 (3)°. In the crystal structure, inter­molecular I⋯N inter­actions [3.099 (4) Å] link hydrogen-bonded aggregates of the hydrozone and solvent molecules related by translation along the b axis into chains. An intramolecular O—H⋯N hydrogen bond forms an S(6) ring. International Union of Crystallography 2011-06-11 /pmc/articles/PMC3151945/ /pubmed/21837030 http://dx.doi.org/10.1107/S1600536811020770 Text en © Sun et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sun, Shan-Shan
Liu, Shi-Yong
Zheng, Ting-Ting
Wang, Xiao-Ling
(E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title_full (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title_fullStr (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title_full_unstemmed (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title_short (E)-N′-(2-Hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
title_sort (e)-n′-(2-hy­droxy-3,5-diiodo­benzyl­idene)nicotinohydrazide acetonitrile monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151945/
https://www.ncbi.nlm.nih.gov/pubmed/21837030
http://dx.doi.org/10.1107/S1600536811020770
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