N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate

The title compound, C(20)H(26)N(4)O(2)·CH(3)OH, was prepared by the reaction of 4-diethyl­amino-2-hy­droxy­benzaldehyde with 4-(dimethyl­amino)­benzohydrazide. The dihedral angle between the two benzene rings is 13.6 (3)° and an intra­molecular O—H⋯N hydrogen bond generates an S(6) ring. In the crys...

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Detalles Bibliográficos
Autores principales: Su, Fu, Gu, Zheng-Gui, Lin, Jun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151952/
https://www.ncbi.nlm.nih.gov/pubmed/21837040
http://dx.doi.org/10.1107/S1600536811019957
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author Su, Fu
Gu, Zheng-Gui
Lin, Jun
author_facet Su, Fu
Gu, Zheng-Gui
Lin, Jun
author_sort Su, Fu
collection PubMed
description The title compound, C(20)H(26)N(4)O(2)·CH(3)OH, was prepared by the reaction of 4-diethyl­amino-2-hy­droxy­benzaldehyde with 4-(dimethyl­amino)­benzohydrazide. The dihedral angle between the two benzene rings is 13.6 (3)° and an intra­molecular O—H⋯N hydrogen bond generates an S(6) ring. In the crystal, the hydrazone and methanol mol­ecules are linked through inter­molecular O—H⋯O and N—H⋯O hydrogen bonds, forming chains along a.
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spelling pubmed-31519522011-08-11 N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate Su, Fu Gu, Zheng-Gui Lin, Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(20)H(26)N(4)O(2)·CH(3)OH, was prepared by the reaction of 4-diethyl­amino-2-hy­droxy­benzaldehyde with 4-(dimethyl­amino)­benzohydrazide. The dihedral angle between the two benzene rings is 13.6 (3)° and an intra­molecular O—H⋯N hydrogen bond generates an S(6) ring. In the crystal, the hydrazone and methanol mol­ecules are linked through inter­molecular O—H⋯O and N—H⋯O hydrogen bonds, forming chains along a. International Union of Crystallography 2011-06-11 /pmc/articles/PMC3151952/ /pubmed/21837040 http://dx.doi.org/10.1107/S1600536811019957 Text en © Su et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Su, Fu
Gu, Zheng-Gui
Lin, Jun
N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title_full N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title_fullStr N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title_full_unstemmed N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title_short N′-(4-Diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
title_sort n′-(4-diethyl­amino-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzo­hydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151952/
https://www.ncbi.nlm.nih.gov/pubmed/21837040
http://dx.doi.org/10.1107/S1600536811019957
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AT guzhenggui n4diethylamino2hydroxybenzylidene4dimethylaminobenzohydrazidemethanolmonosolvate
AT linjun n4diethylamino2hydroxybenzylidene4dimethylaminobenzohydrazidemethanolmonosolvate

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