Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane

The title compound, C(6)H(10)N(8)S(2), was prepared by the nucleophilic substitution reaction of 5-mercapto-1-methyl­tetra­zole and dichloro­ethane. In the crystal, the mol­ecule possesses an approximate non-crystallographic twofold symmetry axis. The crystal packing is stabilized by weak inter­mole...

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Detalles Bibliográficos
Autores principales: Li, Chun-Rong, Chen, Tao, Xia, Zheng-Qiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151974/
https://www.ncbi.nlm.nih.gov/pubmed/21837068
http://dx.doi.org/10.1107/S1600536811021957
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author Li, Chun-Rong
Chen, Tao
Xia, Zheng-Qiang
author_facet Li, Chun-Rong
Chen, Tao
Xia, Zheng-Qiang
author_sort Li, Chun-Rong
collection PubMed
description The title compound, C(6)H(10)N(8)S(2), was prepared by the nucleophilic substitution reaction of 5-mercapto-1-methyl­tetra­zole and dichloro­ethane. In the crystal, the mol­ecule possesses an approximate non-crystallographic twofold symmetry axis. The crystal packing is stabilized by weak inter­molecular C—H⋯N and π–π inter­actions [centroid–centroid distances = 3.448 (6), 3.5085 (5) and 3.4591 (2) Å]. The two five-membered rings form a dihedral angle of 1.9 (2)°.
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spelling pubmed-31519742011-08-11 Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane Li, Chun-Rong Chen, Tao Xia, Zheng-Qiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(6)H(10)N(8)S(2), was prepared by the nucleophilic substitution reaction of 5-mercapto-1-methyl­tetra­zole and dichloro­ethane. In the crystal, the mol­ecule possesses an approximate non-crystallographic twofold symmetry axis. The crystal packing is stabilized by weak inter­molecular C—H⋯N and π–π inter­actions [centroid–centroid distances = 3.448 (6), 3.5085 (5) and 3.4591 (2) Å]. The two five-membered rings form a dihedral angle of 1.9 (2)°. International Union of Crystallography 2011-06-18 /pmc/articles/PMC3151974/ /pubmed/21837068 http://dx.doi.org/10.1107/S1600536811021957 Text en © Li et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Chun-Rong
Chen, Tao
Xia, Zheng-Qiang
Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title_full Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title_fullStr Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title_full_unstemmed Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title_short Bis[(1-methyl-1H-tetra­zol-5-yl)sulfan­yl]ethane
title_sort bis[(1-methyl-1h-tetra­zol-5-yl)sulfan­yl]ethane
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151974/
https://www.ncbi.nlm.nih.gov/pubmed/21837068
http://dx.doi.org/10.1107/S1600536811021957
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AT chentao bis1methyl1htetrazol5ylsulfanylethane
AT xiazhengqiang bis1methyl1htetrazol5ylsulfanylethane

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