7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one

The asymmetric unit of the title compound, C(14)H(10)FN(3)OS(2), contains two independent mol­ecules which differ in the relative orientations of the triazole and allyl­sulfanyl groups with respect to the planar thio­chromen-4-one frameworks. The N—N—C—C torsion angles are 128.2 (5) and −120.9 (5)°,...

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Detalles Bibliográficos
Autores principales: Liu, Dong-liang, Xiao, Tao, Li, Yang, Yu, Guang-yan, Li, Chen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151981/
https://www.ncbi.nlm.nih.gov/pubmed/21837153
http://dx.doi.org/10.1107/S1600536811022665
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author Liu, Dong-liang
Xiao, Tao
Li, Yang
Yu, Guang-yan
Li, Chen
author_facet Liu, Dong-liang
Xiao, Tao
Li, Yang
Yu, Guang-yan
Li, Chen
author_sort Liu, Dong-liang
collection PubMed
description The asymmetric unit of the title compound, C(14)H(10)FN(3)OS(2), contains two independent mol­ecules which differ in the relative orientations of the triazole and allyl­sulfanyl groups with respect to the planar thio­chromen-4-one frameworks. The N—N—C—C torsion angles are 128.2 (5) and −120.9 (5)°, while the C—S—C—S torsion angles are −17.4 (4) and 16.4 (4)°. In the crystal, inter­molecular C—H⋯O and C—H⋯N hydrogen bonds link the mol­ecules in a stacked arrangement along the a axis.
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spelling pubmed-31519812011-08-11 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one Liu, Dong-liang Xiao, Tao Li, Yang Yu, Guang-yan Li, Chen Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(10)FN(3)OS(2), contains two independent mol­ecules which differ in the relative orientations of the triazole and allyl­sulfanyl groups with respect to the planar thio­chromen-4-one frameworks. The N—N—C—C torsion angles are 128.2 (5) and −120.9 (5)°, while the C—S—C—S torsion angles are −17.4 (4) and 16.4 (4)°. In the crystal, inter­molecular C—H⋯O and C—H⋯N hydrogen bonds link the mol­ecules in a stacked arrangement along the a axis. International Union of Crystallography 2011-06-22 /pmc/articles/PMC3151981/ /pubmed/21837153 http://dx.doi.org/10.1107/S1600536811022665 Text en © Liu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Dong-liang
Xiao, Tao
Li, Yang
Yu, Guang-yan
Li, Chen
7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title_full 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title_fullStr 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title_full_unstemmed 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title_short 7-Fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1H-1,2,4-triazol-1-yl)-4H-thio­chromen-4-one
title_sort 7-fluoro-2-(prop-2-en-1-ylsulfan­yl)-3-(1h-1,2,4-triazol-1-yl)-4h-thio­chromen-4-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3151981/
https://www.ncbi.nlm.nih.gov/pubmed/21837153
http://dx.doi.org/10.1107/S1600536811022665
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